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! /41I` 1 <br /> TOXICS LTD. <br /> Laboratory Services Since 1989 <br /> Client Sample ID: SV-1 , <br /> Lab ID#: 1009227ARl-01A <br /> MODIFIED EP MET TO-15 GCIMS <br /> File Name: w091518r1 Date of Collection: 9/9/10 4:30:00 PM ' <br /> Dil.Factor: 2.96 Date of Analysis: 9/15/10 05:24 PM <br /> Rpt. Limit Amount Rpt. Limit Amount <br /> Compound (ppbv) (ppbv) (ug/m3) (ug/m3) <br /> Benzene 15 20 47 62 <br /> Toluene 15 Not Detected 56 Not Detected ' <br /> Ethyl Benzene 15 Not Detected 64 Not Detected <br /> m,p-Xylene 15 Not Detected 64 Not Detected <br /> o-Xylene 15 Not Detected 64 Not Detected ' <br /> Naphthalene 59 Not Detected 310 -Not <br /> TPH ref.to Gasoline(MW=100) 300 250000 1200 1000000 <br /> TENTATIVELY IDENTIFIED COMPOUNDS , <br /> Amount <br /> Compound CAS Number Match Quality <br /> ((ppbv)) <br /> 1-Propene, 1,1,2,3,3,3-hexafluoro- 116-154 53% 4100 NJ ' <br /> Unknown NA NA 4900J <br /> Pentane, 2,4-dimethyl- 108-08-7 91% 6100 NJ <br /> Pentane,2,3-dimethyl- 565-59-3 91% 4100 NJ <br /> Butane,2,2,3,3-tetramethyl- 594-82-1 83% 51000 NJ <br /> Unknown NA NA 4400 J <br /> Pentane, 2,3,4-trimethyl- 565-75-3 91% 26000 NJ , <br /> Pentane, 2,3,3-trimethyl- 560-21-4 90% 30000 NJ <br /> Hexane, 2,2,4-trimethyl- 16747-26-5 83% 6400 NJ <br /> Decane,2,2,5-trimethyl- 62237-96-1 78% 6000 NJ <br /> NJ=The identification is based on presumptive evidence;estimated value. ' <br /> Container Type: 6 Liter Summa Canister(100%Certified) <br /> Method ' <br /> Surrogates %Recovery Limits <br /> 1,2-Dichloroethane-d4 118 70-130 <br /> Toluene-d8 87 70-130 ' <br /> 4-Bromofluorobenzene 103 70-130 <br /> 1 <br /> Page 6 of 12 , <br />