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534 <br /> McCamnbell Analytical. Inc. :www.m=ampbsll.com Pittsburg,CA 9mccarn701 <br /> Web:www.mccampbelLcom E-mail:main t(Jmecampbell.wm <br /> "When Ouality Counts" I Tele hone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/14/08 <br /> • LEARNER Date Received: 05/14/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Mazda Herbert Date Extracted: 05/14/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/20/08 <br /> Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 0805377 <br /> Lab ID 0805377-001A <br /> Client ID 11-1-I <br /> Matrix Soil <br /> R <br /> Comoound Concentration* DF ReL�ng Comoound Concentration* DF ,s <br /> Acetone 0.29 LO 0.05 tett- nnI methyl ether TAME ND 1.0 0.005 <br /> Benzene ND 1.0 0 005 Br m benzen ND I 0.005 <br /> Bromocbioromethane ND 1 0 0 005 BromodichloromethancND <br /> Bromoform ND 1 0 0 005 Bromomethane ND 1.0 0,005 <br /> 2-But n ne MEK ND 1.0 0.02 t-B t I alcohol TBA ND 1.0 0.05 <br /> n-ButvI benzene ND 1 0 0.005 sec-Butyl benzene ND 1.0 0.00 <br /> tert-Butyl benzene N D 1 0 0 005 Carbon Disulficle ND 1.0 0,005 <br /> Carbon Tetrachloride ND 1 hloroben,ene ND 1.0 0,005 <br /> Chlornethane ND 1.0 0.005 Chloroform ND 1.0 0.005 <br /> Chloromethanc ND 1.0 0 005 2- htorotoluene ND 1.0 1 0.005 <br /> 4-Chlorotoluene ND Dibromochlorometbane <br /> 1 - r m - -c r n ND I 4 1 2- EDB ND 1 <br /> Dibr m methane ND 1.0 0 1 2-Diehl r benzen ND 1.0 0.005 <br /> 1-3-Dichlorobenzene ND 1.0 05 1 4-Di hlorobenz ne ND 1.0 0.005 <br /> h1 r diFl h n - i ht r n 10 0,005 <br /> 1 2-Dich h n (1.2-DCA) D 1 1-Di hen. ND 1.0 0,005 <br /> cis-] -Di hI D 1. r - 2-Dich) r n ND I <br /> 1 2-Dichloro ro ne ND 1.0 1 3-Dichloro ro ne ND LO 0. <br /> 2 2-Dich) r ro ane ND 1. 0.005 1.1-Dichloropropene ND Lo 0.005 <br /> 3-Diebloropro,ene ND 1.0 trans-] 3-Dichloro,ropene ND I 0.005 <br /> • Diisouropyl IPE E nz n ND 1. 0 nos <br /> Ethyl tert-but 1 ether ETRE ND 1 0.005 F n 113 ND 1.0 0.1 <br /> Hexachlorobuladiene ND 1.0 0.005 Hexachlor thane ND 1.0 0.005 <br /> 2-Hexanone NQ 1.0n <br /> NQ 1.0 0,005 <br /> 4-Isouropyl toluene ND I M h - 1 ether TBE ND 1.0 0,005 <br /> Methylene chloride ND 1.0 0.00 4-Meth I-2- entanon MIBK ND 1.0 0.005 <br /> Naphthalene ND I.0 0.005 n-Propyl benzene ND 1.0 0,005 <br /> Styrene I 1.2-Tetracbloroetbane ND 1.0 0,005 <br /> 1 1.2.2-Tetratchlorroethane NQ 1.0 Tetrachloroethene NQ 1.0 1 0.0051 <br /> Toluene ND 1 0.005 12 3-Trichl r benzene ND 1 0.005 <br /> 1 2 4-Tri hlorobenzene NDI. 0.00 1 1 1-Trichl roethan ND 1.0 0.005 <br /> 1 hl roethan 1 ND Trichlillgalhene NQ 1 <br /> Trichlorofluoromethane ND 1.0 0.005 1 ? 3-Tricbloronropane NQ 1.0 0.005 <br /> 1.2.4-Trimethylbenzene ND 1.0 0.005 I -Trimeth 1 enzene ND I. 0.005 <br /> Surrogate Recoveries <br /> %SSI. 91 1 ° 2, -77 94 <br /> 0 9 <br /> Comments: <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts <br /> are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> Ill lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)reporting limit raised due to <br /> high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight; <br /> m reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. <br /> • <br /> DHS ELAP Certification No 1644 A: Angela Rydelius,Lab Manager <br />