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McCamnbell Analytical, Inc. 1534 Willa.Pax,Road,Pittsburg,CA 94565-1701 <br /> Web:www,mccampbell.com E-mail:main@mcmmpbell.com <br /> "When Oualiry Counts" Tele hone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/14/08 <br /> • LEARNER Date Received: 05/14/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Marda Herbert Date Extracted: 05/14/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/17/08 <br /> Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 0805377 <br /> Lab ID 0805377-004A <br /> Client ID B-2-5 <br /> Matrix oil <br /> rear"i°sCompound Concentration* DF ayont <br /> rg <br /> Compound Concentration* DF r,;mn ❑m� <br /> Acetone ND 1.0 0.05 tert-Am 1 methyl ether TAME ND I 0.005 <br /> Benzene ND 1.0 0.005 Bromobenzene ND 1.0 0.00 <br /> Bromochlorometbane ND I A n om Bromodichloromethane D 1 0 005 <br /> Bromoform ND 1 0 0 005 Thromomethane ND <br /> 2-Butanon MEK ND I 0. 2 t-But I alcohol TBA ND 1.0 0.05 <br /> n-But I benzene ND I 0 0.005 sec-Butyl benzene ND 1.0 0,005 <br /> tert-flutyl benzene ND 1 0 0.005 Carbon Disulfide1 <br /> Carbon Tetrachloride NQ 1.0 0.005 ChlorobenzeneND 1 <br /> Chl r ethane ND 1.0 0.005 Chloroform ND 1.0 0,005 <br /> Chloromethane ND 1.0 0,005 2- hl rotoluene ND 1.0 0.005 <br /> 4-Chlorotoluene ND 1.0 0,005 Di rm h ND 1.0 0,005 <br /> -Di r - hl r r D 1.0 0,004 1 2-Di h EDB 1.0 0,004 <br /> Di r mome h ne ND 1.0 0,005 1,2-Dichlorobenzene N 1.0 0.005 <br /> 1 3-Dichlorobenzene ND I 0.005 1 4-Dicblorobenzenc ND 1.0 0,005 <br /> Dichlorodifluoromethane D 1.0 0,005 1 1-D chloroetbane1 <br /> 1 2-D' r e h n (1.2-DCA) N Q I1,004 -Di h ne ND 0,005i -1 2-Di D 1 r - -Di hl r n ND 1 0 00512-Dichloro r ne ND 1.0 I -Diehl ro ro ane ND 1.0 5 <br /> 2 2-Dichlor r ane ND 1.0 1 1-Di hloro ro en ND 1.0 05 <br /> ci -1 - I r r n N 1 -I -Di h r n 1r DIPE D h 1 n D I 0.005Eth 1 rbbut I h r ETBE ND 1.0 Freon 113 ND 1.0 0.1 <br /> Hex hl robuta i ne ND 1. Hexachlor thane ND I.0 0.005 <br /> x n ND 1IsoDronvibenzene NQ LO 0,005 <br /> 4-1 1 toluene ND 1 l0,005 1-- ether MTB 1 <br /> Meth 1 ne chloride ND 1 1.0 0.005 4-Meth 1-2- entanone MIBK ND 1 0.005 <br /> N h halene ND 1 0.00 n-Propyl benzene ND 1.0 0,005 <br /> Styrene D 1.0 0,005 1 1.1.?-Tetrachloroetbane ND I <br /> 1.1.2.2-Teirachloroethane N Q 1.0 0,005 Tetrachl r e <br /> Toluene ND 1.0 0,005 12 -TrichIorob nzene ND 1.0 1 0.005 <br /> 1 2 4-Trichloro enzene ND 1.0 0.0 1 I I-Trich I oro eth one ND I 0.005 <br /> i.2-Trichloroethane ND 1.0 0,005 Trichloroethene ND Lo 0.005 <br /> Trichlorofluoromethane ND 1.0 0,005 1 2 3-TrichloroproyaneD I 0.005 <br /> 12 4- rimeth Ibenz ne ND 1.0 .005 1 3 5-Tri h Ibenz n ND 1.0 5 <br /> Surrogate Recoveries <br /> 4 ° <br /> Comments: <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts <br /> are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> h)lighter than water immiscible sheen/product is present;it liquid sample that contains greater than-1 vol.%sediment;it reporting limit raised due to <br /> high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight; <br /> m)reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. <br /> • <br /> DHS ELAP Certification No 1644 Angela Rydelius,Lab Manager <br />