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McCampbell Analytical, Inc. 1534 Will. Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mecampbell.com E-mail:main@mccampbell.com <br /> "When Oualim Counts" Telephone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/14/08 <br /> • LEARNER Date Received 05/14/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Marda Herbert Date Extracted 05/14/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/16/08-05/21/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805377-020E 0805377-021E 0805377-022E 0805377-023E Reporting Limit for or 1; <br /> Client I B-1 B-2 B-3 B-4 No means not detected <br /> above the reporting limit <br /> Matrix W W W W s w <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/kg pg/L <br /> ICP-MS Metals,Concentration* <br /> An Iv' a ethnd: E200.8 Extraction Method E200R Work Order: 0805377 <br /> Dilution Factor 1 20 1 1 1 1 I 1 I 1 I <br /> Antimony ND<10 ND ND 0.57 NA 0.5 <br /> Arsenic 210 150 190 55 NA 0.5 <br /> Barium 11,000 3600 5300 970 NA 5.0 <br /> Beryllium 16 4.7 6.6 1.3 NA 0.5 <br /> Cadmium 92 7.1 7.7 1.9 NA 0.25 <br /> Chromium 610 240 340 96 NA 0.5 <br /> Cobalt 410 170 310 42 NA 0.5 <br /> Copper 2900 490 810 210 NA 0.5 <br /> Lead 7100 370 470 120 NA 0.5 <br /> Mercury 15 0.48 1.3 0.30 NA 0.012 <br /> Molybdenum 11 10 4.2 22 NA 0.5 <br /> Nickcl 1200 310 520 110 NA 0.5 <br /> Selenium ND<10 2.4 3.5 1.2 NA OS <br /> Silver 7.9 0.99 2.5 0.40 NA 0.19 <br /> Thallium ND<10 3.9 5.5 0.67 NA 0.5 <br /> Vanadium 920 620 950 200 NA 0.5 <br /> Zinc5 0 2000 3900 690 NA .0 <br /> 99 9 103 <br /> Comments it <br /> -water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,filter samples in pg/filter. <br /> #means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> it aqueous sample containing greater than-1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrogate recovery, <br /> caused by matrix interference;n results are reported on a dry weight basis see attached narrative. <br /> • DHS ELAP Certification No 1644 `` Angela Rydelius,Lab Manager <br />