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34 <br /> CA <br /> MCCampbell Analytical, Inc. 5a,w.mcowPass Road,Pg,ain@mc 5-1701 <br /> �^ Web:www.mccampbell.com E-mail:&maiinain@mc�inpbell.com <br /> 4;4 "When Quality Counts" I Telephone:877-252-9262 Pax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRL05; Date Sampled: 05/14/08 <br /> • 315 W.Pine Street,Suite 8 LEARNER Date Received 05/14/08 <br /> Client Contact: Mazda Herbert Date Extracted 05/14/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/17/08-05/20/08 <br /> CAM/CCR 17 Metals* <br /> Lab ID 0805377-006A 0805377-007A 0805377-009A 0805377-OIOA Repmong Limit for DF-I <br /> Client ID B-3-1 B-3-5 B4-1 B-4-5 ND means not detected <br /> above the reporting limit <br /> Matrix S S S S S w <br /> Extraction Type TOTAL TOTAL TOTAL TOTAL mg/ICg mg/L <br /> ICP-MS Metals,Concentration* <br /> Analytical Method: 6020A Extraction Method: SW3050B Work Order: 0805377 <br /> Dilution Factor I I 1 I I I <br /> Antimony 61 ND 28 ND 0.5 NA <br /> Arsenic 18 19 22 21 0.5 NA <br /> Barium 430 190 340 730 5.0 NA <br /> Beryllium ND 0.54 ND 0.62 0.5 NA <br /> Cadmium 19 ND 18 ND 0.25 NA <br /> Chromium 420 48 190 52 0.5 NA <br /> Cobalt 24 11 17 36 0.5 NA <br /> Copper 800 29 1400 31 0.5 NA <br /> Lead 2000 1 7.0 3000 8.8 0.5 NA <br /> Mercury 3.1 ND 2.0 ND 0.05 NA <br /> Molybdenum 34 0.51 22 1.1 0.5 NA <br /> Nickel 260 38 170 46 0.5 NA <br /> Selenium NO ND ND NO 0.5 NA <br /> • Silver 1.1 ND LI NO 0.5 NA <br /> Thallium ND NO ND NO 0.5 NA <br /> Vanadium 42 95 52 150 0.5 NA <br /> 7. 00 62 4 20 5 <br /> : 105 NA <br /> %S 106 1 I1 <br /> Comments <br /> -water samples are reported in pg/L,product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in <br /> mg/L,soil/sludge/solid samples in mg/kg wipe samples in pg/wipe,filter samples in pg/filter. <br /> 9 means surrogate diluted out of range;ND means not detected above the reporting limit;N/A means not applicable to this sample or <br /> instrument. <br /> TOTAL=acid digestion. <br /> WET=Waste Extraction Test(STLC). <br /> DI WET=Waste Extraction Test using de-ionized water. <br /> i)aqueous sample containing greater than—1 vol.%sediment;for DISSOLVED metals,this sample has been preserved prior to filtration;for <br /> TOTAL metals,a representative sediment-water mixture was digested;j)reporting limit raised due to insufficient sample amount;J)analyte <br /> detected below quantitation limits;k)reporting limit raised due to matrix interference;m)estimated value due to low/high surrrogate recovery, <br /> caused by matrix interference;n results are reported on a dry weight basis see attached narrative. <br /> • DHS ELAP Certification NO 1644 ---Angela Rydelius,Lab Manager <br />