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McCampbell Analytical, Inc. 534 W i11ow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:mainiumccampbell.com <br /> 'When Quality Counts" Telephone:877-252-9262 Fax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05;Learner Date Sampled: 05/15/08 <br /> • Date Received: 05/15/08 <br /> 315 W.Pine Street,Suite 8 <br /> Client Contact: Mazda Herbert Date Extracted: 05/15/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/16/08 <br /> Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW5030B Analytical Method: SW8260B Work Order: 0805420 <br /> Lab ID 0805420-013A <br /> Client ID B-13-5 <br /> Matrix Soil <br /> Repartin6Reporting <br /> Compound Concentration* DF �;m;t Comoound lConcentration*1 DF Limit <br /> Acetone ND 1.0 0 05 tcrt-Amvl meth I ether TAME ND 1.0 0.005 <br /> Benzene ND 1.0 0 005 Fromobenzene ND 1.0 0.005 <br /> Bromochloromethane NQ 1 Bromodichloromethane ND Lo 0,005 <br /> Bronnoform ND lo 0,005 Bromomethane ND 1.0 0,005 <br /> 2-B none MEK ND 1.0 0,02 t-But 1 alcohol TBA ND 1.0 0.05 <br /> n-Bu[ I benzene ND 1.0 0.005 sec-putyl benzene ND I .005 <br /> tert-Butyl benzene ND Lo 0,005 Carbon Disulfide ND <br /> Carbon Tetrachloride ND 1.0 0,005 ChlorobenzeneND I <br /> Chi oroethane ND I.0 0.005 Chloroform ND 1.0 0.005 <br /> Chloromethane ND 1.0 0.005 2-Chlorotoluene ND 1.0 0.005 <br /> 4-Chlorocoluene NQ 1 0 0 005 1 Dibromochloromethane NQ Lo 0.005 <br /> 1 2-D' - h nj00 r m EDB ND I 4 <br /> Dibrom methane ND M.0 <br /> 1 2-Di hlorobenzen ND 1.0 .005 <br /> 1 3-Dichlorobenz n ND 1 4-Dichloro nz ne ND 1.0 0.005 <br /> r i h n ND -D' hI r n ND I 01 2-Di h n 1 2-D 11- h ne 1 0 0,005cis- 2-Di hlor t ND -1 2-Di hl n D 1.0 0,0051 2-Dichloro ro ane ND 1 -Dichloro ro ne ND 1 .005 <br /> 22-Dichlor r ane ND I 1-Diehl r ro ene ND 1.0 0.0051 <br /> • cis-is - r r F n - hl r 1 <br /> Dii 1 ether E nND 1.0 0,005 <br /> Eth I t r-but 1 ether ETBE ND 1.0 0.005 1 Freon 113 ND 1.0 0.1 <br /> Hexa hl robutadiene ND 1. 0.005 H x chloroeth ne ND 1.0 0.005 <br /> 2-Hexanone ND 1.0 0.005 TsoDrocvlbcn=e ND 1.0 M05 <br /> 4-Isonropyl toluene ND 1 h1- - hr M 1.0 0,005 <br /> Meth Iene chloride ND 1.0 0.0 4-Meth 1-2- entanone MIRK D 1.0 0,005 <br /> Naphthalene ND 1.0 0.005 n-Propyl benzene ND 1 0.005 <br /> Styrene ND 1.0 0,005 1.1.1.2-Tetrachloroethanc ND <br /> 1.1-2-2-Tetrachloroethane ND 1 Tetrachloroetbene ND 1 <br /> Toluene ND 1 0.005 1 2 3-Trichloro nzene ND 1.0 0.005 <br /> 1.2.4-Trichlorobenzene ND LO 0,005 1 1 1-Trichloroethane ND 1. 0.005 <br /> 1 1.2-Trichloroetbane NQ 1 .005 Trichloroethene D 1.0 0.005 <br /> Trichlorofluoromethane ND L0.005 1 - h r n ND I 0,005 <br /> 1 2 4-Trimeth (benz n ND 1. 0.005 1 -Trimeth I nzene ND 1.0 0,005 <br /> XvIenes <br /> Surrogate Recoveries 103 <br /> gComments: 96 2. <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP extracts <br /> are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;it reporting limit raised due to <br /> high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight; <br /> m)reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. <br /> • <br /> DHS FLAP Certification N° 1644 Angela Rydelius,Lab Manager <br />