Laserfiche WebLink
MCCamDbellAnalytical, InC 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> s We b:www.mccampbell.com E-mail:main@mccampbell.com <br /> "When Orality Cconts° Telephoto-877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8270C <br /> W.O.Sample Matrix: Soil QC.Matrix: Soil - WorkOrder 0805420 <br /> EPA Method SW8270C Extraction SW3550C BatchlD: 35674 Spiked Sample ID: 0805420-073A <br /> AnalY to Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg mg/Kg %Rec. %Rec. %RPD %Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> Acenaphthene NO 2 68.7 68.7 0 64.8 63.4 2.23 30- 130 30 30- 130 30 <br /> 4-Chloro-3-methylphenol NO 4 65.9 64 2.82 78.8 74.3 <br /> 5.86 30- 130 30 30- 130 30 <br /> 2-Chlorophenol ND 4 69.2 65.9 4.84 74.5 73 1.99 30- 130 30 30- 130 30 <br /> 1,4-Dichlorobenzene NO 2 74.5 72.4 2.87 66.8 66.5 0.465 1 30- 130 30 30- 130 30 <br /> 2,4-Dinitrotoluene ND 2 62.4 59.7 4.42 58.4 55.4 5.18 30- 130 30 30- 130 30 <br /> 4-Nitro hent NO 4 58 58.7 1.05 78.1 74.6 4.62 30- 130 30 30- 130 30 <br /> N-Nitrosodi-n-propylamine ND 2 59.6 57.4 3.67 68.8 68.2 0.803 30- 130 30 1 30- 130 1 30 <br /> Pentachlorophenol NO 4 47.6 48.6 2.11 57.4 52.6 8.61 30- 130 30 1 30- 130 30 <br /> Phenol ND 4 60.1 57.9 3.65 86.5 84.5 2.26 30- 130 30 30- 130 30 <br /> Pyrene NO 2 63.2 58.3 7.95 67.4 66.1 1.90 30- 130 30 30- 130 30 <br /> 1,2,4-Trichlorobenzene ND 2 73.1 70.1 4.18 73.7 72.1 2.18 30- 130 30 30- 130 30 <br /> %SSI: 80 200 85 82 2.85 95 93 2.18 30- 130 30 30- 130 30 <br /> %SS2: 81 200 83 81 3.05 104 102 2.00 30- 130 30 30- 130 30 <br /> %SS3: 74 200 78 74 6.20 100 97 2.56 30- 130 30 30- 130 30 <br /> %SS4: 95 200 1 98 97 0.817 80 79 0.973 30- 130 30 30- 130 30 <br /> AIIIL%SSS: 80 200 76 73 4.14 112 107 4.09 30- 130 30 30- 130 30 <br /> %SS6: 84 200 80 72 10.8 85 84 1.32 30- 130 30 30- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35674 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805420-OOIA 05/15/08 10:15 AM 05/15/08 05/18/08 2:55 PM 0805420-002A 05/15/08 10:25 AM 05/15/08 05/22/08 5:39 AM <br /> 0805420-003A 05/15/08 10:30 AM 05/15/08 05/18/08 8:21 AM 0805420-004A 05/15/08 10:45 AM 05/15/08 05/22/08 9:16 AM <br /> 0805420-005A 05/15/08 10:55 AM 05/15/08 05/18/08 9:37 AM 0805420-006A 05/15/08 11:30 AM 05/15/08 05/22/08 10:30 AM <br /> 0805420-007A 05/15/08 11:40 AM 05/15/08 05/18/08 10:54 AM 0805420-OO8A 05/15/08 11:35 AM 05/15/08 05/18/08 12:14 PM <br /> 0805420-009A 05/15/08 12:00 PM 05/15/08 05/18/08 1:34 PM 0805420-OIOA 05/15/08 12:10 PM 05/15/08 05/19/08 11:28 AM <br /> 0805420-011A 05/15/08 1:15 PM 05/15/08 05/18/08 7:06 AM 0805420-012A 05/15/08 1:45 PM 05/15/08 05/19/08 12:47 PM <br /> 0805420-013A 05/15/08 2:05 PM 05/15/08 05/18/08 3:25 AM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Central Sample;LCSD=Laboratory Central Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100-(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> #)surrogate diluted out of range;8=low or no recovery of surrogate or target analytes due to matrix interference. <br /> .laboratory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels. <br /> DHS ELAP Certification No 1644 J2- QA/QC Officer <br />