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MCCamAbellAnalytical Inc 1534 Willow Pass Road,Pittaborg,CA94565-1701 <br /> F^ Web:www.mccampbell.com E-mail:main@mccampbell.com <br /> 'When Quality Counts" Tele hone:877-252-9262 Fax 925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8015C <br /> - W.O.Sample Matrix: Water QC Matrix: Water WorkOrder 0805420 <br /> EPA Method SW8015C Extraction SW3510C BatchlD: 35667 Spiked Sample ID: N/A <br /> Analyte Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> pg/L pg/L %Rec. %Rec. %RPD % Rec. %Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> TPH-Diesel(C 10-C23) N/A 1000 N/A N/A N/A 128 129 0.664 N/A N/A 70- 130 30 <br /> %S8 N/A 2500 N/A N/A N/A 104 105 0.727 N/A I N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35667 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805420-014A 05/15/08 2:50 PM 05/15/08 05/17/08 8:35 AM 0805420-OISA 05/15/08 3:00 PM 05/15/08 05/17/08 9:41 AM <br /> 0805420-016A 05/15/08 3:15 PM 05/15/08 05/20/08 4:01 PM 0805420-017A 05/15/08 3:35 PM 05/15/08 05/17/08 11:55 AM <br /> 0805420-018A 05/15/08 3:50 PM 05/15/08 05/20/08 7:35 PM 0805420-019A 05/15/08 4:10 PM 05/15/08 05/17/08 3:16 PM <br /> • <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for sail matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 QA/QC Officer <br /> • <br />