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McCamnbell Analytical, Inc. 1534 Will..Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mecmnpbell.com E-mail:mainLmccampbell.com <br /> "When Owdity Counts" Telephone:877-252-9262 Pax:925-252-9269 <br /> WGR Southwest,Inc. Client Project ID: #704.PRI.05; Date Sampled: 05/16/08 <br /> • <br /> 315 W.Pine Street,Suite 8 LEARNER,2711 Navy Dr.,Stockton,Ca Date Received: 05/16/08 <br /> Client Contact: Marda Herbert Date Extracted: 05/16/08 <br /> Lodi,CA 95240 Client P.O.: Date Analyzed 05/19/08 <br /> Volatile Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method: SW50300 Analytical Method: SW8260B Work Order: 0805464 <br /> Lab ID 0605464-006A <br /> Client ID B-16-5 <br /> Matrix oil <br /> Comoound Concentration• DF R`Urn�ag * RvPm it <br /> umh Comoound Concentration DF �,m;, <br /> Acetone ND 1.0 0.05 terr-Amy]methyl ether(TAME) ND 1.0 0.005 <br /> Benzene ND 1.0 0.005 Bromobenzene ND 1.0 0.005 <br /> Bromochloromethane N D 1 Bromodichloromethane N <br /> Br nnf rm ND I Brarommethane ND 1.0 0,005 <br /> 2-B t none MEK ND 1.0 0.02 1 t-Bu I alcohol TBA ND 1 0.05 <br /> n-Bu[ I benzene ND 1.0 0.005 sec-Bulyl benzene ND 1.0 0.005 <br /> tert-Bulyl benzene ND I D I <br /> Carbon Tetrachloride ND D 1 <br /> Chloroethane ND 1.0 0.005 Chloroform ND 1.0 0.005 <br /> Chloromethane ND 1.0 0.005 2-Chloro[ luene ND 1.0 0.005 <br /> 4-ChlorotoInerve ND 1 Dibromochloromethare, <br /> 1.2-Dibromo-3-chloropropane ND 1 4 1 2-Di r m h n D ND 1.0 0,004 <br /> Di romomethane ND 1.0 0.005 1 2-Dichlorobenzene ND 1 0.005 <br /> 1.3-Dichlorobenzene ND 1.0 0.005 1.4-Dichlorobenzene ND 1 0.005 <br /> Dichlorodifluoromethane 11-Diehl r eth ne ND 1 <br /> 1.2-Dichloroethane(I.2-DCA) ND 10,004 11-Diehl r ethene NQ 1 <br /> cis-I - i hl ND h ne ND 1.0 0,005 <br /> 1 2-Dichloro ro ane ND 1 1.3-Dichloropronane ND 1.0 1 0.005 <br /> 2 2-Dichloro ro ane ND 1.0 0.005 1 1-Dichloro ro ene ND 1.0 0.005 <br /> • cis-13-Dichloro ro ene ND 1,0 0.005 trans-1 - i hl r r 1.0 0,005 <br /> Diisopropyl ether DIPE NQ 1.0 0.005 Ethvlbenzene NQ 1.0 0.005 <br /> Ethyl ert-but I ether ETBE ND 1. 05 Freon 11 ND I 0 0.1 <br /> Hexa hl r utadiene ND 1. Hexachl r ethane ND I. 0.005 <br /> N nz n <br /> 4- ND ether D 1.0 0,005 <br /> Methylene chloride ND 1. 4-Meth I-2- entanone MIBK ND 1.0 0,005 <br /> Naphthalene ND 1.0 0.005 n-Pro 1 benzene ND 1 0.005 <br /> Styrene N 1. 1 1 1 2-Tetrhloroethane ND <br /> 1.1.2.2-Tetrachloroethane 1 5 T r hl r hene, ND 1.0 0,005 <br /> Toluene ND 1.0 0.005 1 2 3-Trichlorobenzene ND I .005 <br /> 1 2 4-Trichlorobenzene ND 1.0 0.005 1.1.1-Trichloroethane ND 1.0 0.005 <br /> 1.1.2-Trichloroethane ND 1 0.005 Trichloroethene ND 1.0 0,005 <br /> Trichlorofluoromethane ND 1 0.005 1.2.3-Trichloropropane ND 1.0 0,005 <br /> 1 2 4-Trimeth (benzene ND 1.0 0.005 1 3 5-Trimeth (benzene ND 10.005 <br /> Surrogate Recoveries <br /> ° 94 93 <br /> 93 <br /> Comments: <br /> *water and vapor samples are reported in pg/L,soil/sludge/solid samples in mg/kg product/oil/non-aqueous liquid samples and all'rCLP&SPLP extracts <br /> are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or coelutes with another peak;&)low surrogate due to matrix interference. <br /> Fit lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment;j)reporting limit raised due to <br /> high organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight; <br /> m)reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. <br /> DHS ELAP Certification No 1644 J2- Angela Rydelius,Lab Manager <br />