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MCCamAbellAnalytical, Inc 1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mccampbell.com E-mail:main@mocampbell.com <br /> "When Ouslity I Tele hone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SM5520E/F <br /> W.O.Sample Matrix: Soil OC Matrix: Soil WorkOrder 0805464 <br /> EPA Method SM5520E/F Extraction SM5520E/F BatchlD: 35715 Spiked Sample ID: 0805464.009A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> mg/Kg ni %Rec. %Rec. %RPD %Rec. %Rec. %RPD I MS/MSD RPD LCS/LCSD RPD <br /> POO ND 1000 106 109 3.53 107 103 4.13 70- I30 1 30 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br /> NONE <br /> BATCH 35715 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805464-OOIA 05/16/08 8:05 AM 05/16/08 05/20/09 12:10 PM 0805464-003A 05/16/08 8:15 AM 05/16/08 05/20/09 12:15 PM <br /> 0805464-OOSA 05/16/08 8:35 AM 05/16/08 05/20/09 12:20 PM 0805464-007A 05/16/08 9:15 AM 05/16/08 05/20/09 12:25 PM <br /> 0805464-009A 05/16/08 9:40 AM 05/16/08 05/20/09 12:30 PM <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS t MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance coterie due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyto concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 J2— QA/QC Officer <br />