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1534WillowPassRoad,Pittsburg,CA 94565-1701 <br /> McCamubell Analvtical, Inc. <br /> Web:www.mccampbell.com E-mail:mainQamccampbell.com <br /> "Whey Oualim Counts' I Tele hone:877-252-9262 Fax:925-252-9269 <br /> QC SUMMARY REPORT FOR SW8082A <br /> W.O.Sample Matrix: Soil 'OC Matrix: Soil WorkOrder 0805464 <br /> EPA Method SW8082A Extraction SW3550C BatchlD: 35675 Spiked Sample ID: 0805420.013A <br /> Analyte Sample Spiked MS I MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> Mg/kg mg/kg %Rec. %Rec. %RPD N.Rec. %Rec. %RPD MS/MSD RPD LCS/LCSDRPD <br /> Aroclor1260 NO 0.075 193171 194FI 1.85 126 125 0.531 70- 130 20 70- 130 20 <br /> %SS: 99 0.050 119 123 3.76 82 81 0.590 70- 130 20 70- 130 20 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the method RL with the following exceptions: <br /> NONE <br /> Fl =MS/MSD outside of acceptance criteria.LCS-LCSD validate prep batch. <br /> BATCH 35675 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805464-OOIA 05/16/08 8:05 AM 05/16/08 05/21/08 3:08 AM 0805464-002A 05/16/08 7:55 AM :05/16/08 <br /> 08 05/18/08 12:32 AM <br /> 0805464-003A 05/16/08 8:15 AM 05/16/08 05/21/08 4:03 AM 0805464-004A 05/16/08 8:35 AM 05/18/08 1:28 AM0805464-005A 05/16/08 8:35 AM 05/16/08 05/21/08 4:57 AM 0805464-006A 05/16/08 9:00 AM08 05/18/08 3:19 AM0805464-007A 05/16/08 9:15 AM 05/16/08 05/21/08 7:41 AM 0805464-008A 05/16/08 9:35 AM08 05/18/08 2:23 AM <br /> 0805464-009A 05/16/08 9:40 AM 05/16/08 05/20/08 5:57 PM <br /> i <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification 1644 Ok_ QA/QC Officer <br /> 0 <br />