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McCamnbell Analytical, Inc. 1534 Wine.Pass Road,Pittsburg,CA 94565-1701 <br /> Web:www.mc pbell.com E-mail:main@mccampbell.com <br /> "When Ouality Counts" I Telephone,877-252-9262 Fax:925-252-9269 <br /> • QC SUMMARY REPORT FOR SW8082A <br /> W,O.Sample Matrix: Water OC Matrix: Water WorkOrder: 0805464 <br /> EPA Method SW8082A Extraction SW3510C BatchlD: 35644 Spiked Sample ID: N/A <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) <br /> pg/L pg/L %Rec. % Rec. %RPD % Rec. % Rec. %RPD MS/MSD RPD LCS/LCSD RPD <br /> AToclor1260 N/A 3.75 N/A N/A N/A 88.2 91.2 3.36 N/A N/A 70- 13020 <br /> %SS: N/A 2.5 N/A N/A N/A 114 108 5.64 N/A N/A 70- 130 30 <br /> All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the fallowing exceptions: <br /> NONE <br /> BATCH 35644 SUMMARY <br /> Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br /> 0805464-OTIC 05/16/08 10:45 AM 05/16/08 05/20/08 5:02 PM 0805464-012C 05/16/08 11:15 AM 05/16/08 05/20/08 4:06 PM <br /> 0805464-013C 05/16/08 11:30 AM 05/16/08 05/18/08 7:02 AM 0805464-014C 05/16/08 11:45 AM 05/16/08 05/18/08 8:53 AM <br /> 0 <br /> MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. <br /> %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100`(MS- MSD)/((MS•MSD)/2). <br /> MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix Interferes with the spike recovery. <br /> N/A=not enough sample to perform matrix spike and matrix spike duplicate. <br /> NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br /> DHS ELAP Certification No 1644 JVI_ QA/QC Officer <br /> 0 <br />