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Lancaster <br /> Laboratories r4nalysis Report <br /> 3 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425.717-656.2900 Fax:717-656-2681•www.lancasteriabs.com <br /> Pagel of 3 <br /> Quality Control Summary <br /> f. . Client Name: ChevronTexaco Group Number: 872571 I I <br /> Reported: 11/07/03 at: 10 :51 AM <br /> Laboratory Compliance Quality Control. <br /> 13 <br /> Blank Blank Report LCS LCSD LCS/LCSD €i <br /> Aaalysi8 Name Result MDL Units %REC %REC- Limits RPD RPD Max . <br /> Batch number: 03301A51A Sample number(s) : 4152615-4152625 <br /> TPH-GRO - Waters N.D. 50. ug/l 88 103 70-130 15 30 44 <br /> Batch number: 033070007A Sample number(s) : 4152624-4152625 P <br /> Methanol (by Direct Injection) N.D. 1000. ug/l 96 78-114. <br /> ;I <br /> Batch number: P033024AA Sample number(s) 4152614-4152620 <br /> Methyl Tertiary Butyl Ether N.D. 2. ug/l 99 77-127' i <br /> Benzene N.D. .5 ug/l 103 85-117 <br /> Toluene N.D. .5 ug/l 103 85-115 <br /> Ethylbenzene N.D. .5 ug/l 102 82-119 <br /> Xylene (Total) N.D. .5 ug/1 104 84-120 <br /> Batch number: P033031AA Sample number(s) : 4152624-4152625 <br /> Ethanol N.D. 500. ug/l 89 46-145 J <br /> Methyl Tertiary Butyl Ether N.D. 2, ug/l 95 77-127 <br /> di-Isopropyl ether N.D. 2, ug/l 93 74-125 <br /> Ethyl t-butyl ether N.D. 2. ug/l 90 74-120 <br /> 't-Amyl methyl ether N.D. 2. ug/1 95 79-113 <br /> 't-Butyl alcohol N.D. 100. ug/1 101 53-147 <br /> ..Benzene N.D. .5 ug/1 95 85-117 <br /> 1-Dichloroethane N.D. 2. ug/l 94 77-132 <br /> iuene N.D. .5 ug/1 93 85-155 <br /> 2-Dibromoethane N.D. 2. ug/l 92 81-114 <br /> Ethylbenzene N.D. .5 ug/1 93 82-119 <br /> Xylene (Total) N.D. .5 ug/l 95 84-120 <br /> Batch number: P023032AA Sample number(s) : 4152621-4152623 <br /> Methyl Tertiary Butyl Ether N.D. 2, ug/l 98 77-127 <br /> Benzene N.D. .5 ug/l 101 85-117 <br /> Toluene N.D. .5 ug/l 104 85-115 <br /> Ethylbenzene N.D. .5 ug/1 103 82-119 <br /> Xylene (Total) N.D. 5 ug/l 105 84-120 I <br /> I al I <br /> Sample Matrix Quality Control <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup, <br /> RPD <br /> Analysis Name %REC %REC Limits RPD MAX Cone Cone RPD Max,. <br /> ,Batch number: 03301A51A Sample number(s) : 4152615-4152625 <br /> :TPH-GRO - Waters 99 63-154 " <br /> .Batch number: 033070007A Sample number(s) : 4152624-4152625 <br /> Methanol (by Direct Injection) 104 104 73-117 0 20 tt <br /> Batch number: P033024AA Sample number(s) : 4152614-4152620 i r <br /> Methyl Tertiary Butyl Ether 100 100 69-134 0 30 <br /> Benzene 107 106 83-128 1 30 <br /> 'Toluene 108 110 83-127 1 30 <br /> -Ethylbenzene 109 111 82-129 2 30 <br /> Xylene (Total) 110 112 82-130 2 30 <br /> ,Batch number: P033031AA Sample number(s) : 4152624-4152625 <br /> *-Outside of specification f. <br /> 1 The result for one or both determinations was less than five times the LOQ. <br /> ) The background result was more than four times the spike added. <br /> f <br />