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's <br /> i <br /> r SUPERIOR ANALYTICAL LABORATORY, PNC, <br /> t r5 BURKE, UNIT I. SAN FRANCISCO,CSA 94124 ' PHONE <br /> 415 647 20B1 <br /> i5» . S I <br /> - I C A T E O <br /> F <br /> A <br /> N a, L <br /> Y <br /> t R T I f <br /> C E <br /> 1 <br /> LABORATORY N0. 52344-2 DATE RECEIVED: 06/06/90 <br /> CLIENT: Sierra Environmental DATE REPORTED: 08/13/80 <br /> Services JOB NO. 1-146-00 <br /> EPA SW-846 METHOD 8240 - VOLATILE ORGANICS <br /> by Gas Chromatography/ Masc Spectrometry <br /> SAMPLE: MW5-15.5 <br /> u5/kg Compound u9/k9 <br /> Compound __--__ ----- <br /> --- - ND<15 <br /> Chloromethane ND<50 Cis-1 ,3-Dichioropropene ND<15 <br /> Bromomethaltie ND<50 Trichloroethene 14D<15 ND <br /> Vinyl chloride <br /> ND<50 Dibromochloromethane <15 <br /> Chlarodth�!ne ND<50 1 ,1 ,2-Trichlaraethane <br /> MethYiene Chloride ND<50 ;BerlZene'r ND<i5 <br /> ND<50 -Trans-l ,3-bichloropraPene ND<15 <br /> Acetone <br /> Carbon ;iisulfide ND<15 2-Chloroethyl vinyl ether ND<15 <br /> TrichloralzlLoiomethane ND<15 Bramoform ND<50 <br /> . 1 ;1-Dichloroethene ND<15 4-Methyl-2-Pentanone ND<50 <br /> i ,1--Dichlor.oethane ND<15 Z-Wexanane ND<15 <br /> 1 ,2-Dichloroethsne (total ) ND<15 TetrachloroeND<15 <br /> thene <br /> Chloroform ND<15 1 ,1,2,2-Tetrachloroethane Ni7.<.15 <br /> t .2-Dichloroethane ND<15 Toluene ND<15 } <br /> ND<100 Chlorobenzene <br /> 2-Sutanone NDt1:5 <br /> 1 ,2 ,1-Trichloroethane ND<15 •,Et4klbenzene ND<15 <br /> Carbon Tetrachloride ND<15 Styrene ND<1'5 <br /> Vinyl Acetate ND<50 Tota'. Xylones ND<15 l <br /> IBramodiehioromethane ND<15 . 13=Dichlorobenzene ND<15 . <br /> 1 ,2-a7ichloroprovene ND<15 <br /> 1,2&1 ,4-Dichlorobenzenes s <br /> l.. ug/kg = Pert per billion (ppb) <br /> 4C DATA: QC Limits <br /> Surrogate Recoveries water soil <br /> 76-114 81-117 <br /> 1 ,2-DCA-d4. . . .. . . . . . . . . . 103%% 88-110 81-140 <br /> Tolueno-d8. . . . . . . . . . . . . . 86-115 74-121 <br /> Bromofluorobenzene. . . . . . 10115 <br /> r <br /> comments: Ric rd Srna, Ph.D. <br /> Laboratory Director <br /> OWSTANDING QUALITY AND SERVICE <br />