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/ McCamobell Analytical, Inc. 1134WivawPassRo.&Nishing.(-A94S65-1701 Wetr.truvt:mreamphellcom li-mail.main(a iruampkllrom "ll'ben Oualilc Chums" Tele hone e77-2S2A262 Fa, 915-252-9269 • WGR Soulhwest.Inc. Cliem Project ID: 4773.1111.02 Date Sampled: 10/03/07 +15 V', fine Street Suite R Date Received: 10'0;'07 Client Contact: Caryl Sheehan Date Extracted: 10/03/07 Lodi,CA 95240 Client P.f 1: Date Analyzed: 10/04/07 Volatile Organic%by PXT and GC/MS(Basic Target List)* I.xtruanun 51ethoJ. SN ttr:OB nnulnmul llcthod 1Wx260R N'mkOrdct. 0710131 Lab 11) 0710131-004A Client 11) 134 Matrix Soil Comnound Concentration' DP nOr,,,� t Comnound Gmcentrauon Acetone ND 1.0 0.05 Acrolein pro enal ND 1.0 0.05 Acrvlonitrile ND 1.0 0.02 ler[-Am l methyl ether TAME ND 1.0 0005 Benzene ND 1.0 0.005 Bromoben2ene ND 1.0 O.UUS Bromochloromethane ND 1.0 0.005 Brnmodichloromethane ND 1.0 0.005 Hromolorm ND 1.0 0,005 JiTornomethine N) 1.0 ( 005 ''-filum n N) 1.0 0.0' i-Butyl a N) 1.0 OU .-Butyl IiCI17COC Nil 1.0 0.005sec- t l bertzene N) Lo 0,005 tert-Butyl benzene NQ 1.0 O.UOS Carbon )is Ih e ND 1.0 W005 Carbon etrachloride Nil IM QUOS Chlorohen7enc Nil 1.fl 1.105 Chlo'cellumc ND 1.0 0.005 12C e0 •1 Vinyl Ether Nil 1.0 0.01 Chloroform ND 1.0 0.005 1 Chli,omethmicND 10 0,005 I I...owlucue Nil i 1) 0.005 14-C' I atoluene N) 1.0 0.005 ibio hoc I et to a Nil 11) 0.00e ib o-T_ to 0 o'a N) 1,0 0.005 '- )fibro net a E 0 0.005 1 Dihona,methane Nil 1.0 O Is I '-1 is r o ober e N 0 0.005 1 1 I-Do,lilotolien7enc Nil J'O 0,00 4-S darnbc zNil 1.0 0.005 1 Dichl.,ndifluoromethane0 0,905 11- )ie t n oct a - ND Lo 0.005 1 1 '-Diel to et r rte ,-DCA) ' .0 0.005 • 11- is n oct • NI .0 O.OUS Icis-1 '- icl for et enc NQ 1 0 -0,00, lrm,,-l.'-DichlorQcIhcnc Nil IM 0.005 1 1 2- '•I to r ro ate N .0 0,005 1-3-Dichloro ro ane ND 1.0 0005 1 ' 2-Dichloro ro ane ND I.0 0.005 1 1-Dichloro roene ND Lu 0.005 1 cis-1 3-Dichloro,ro rene ND 1.0 0.005 trans-1 3-Dichloro ro ene ND 1.0 0.005 1 Diiso rocl ether DIPS ND LO 0-005 Ethvlbemenc ND LU 0.005 1 Elhrl reit-bulvl ether ETRE NL) LO 0.005 Freon 113 ND jOn .1 Hexachlorobutadicne ND 1.0 0.005 Hexachloroethane ND 005 2-Hexanonc ND 1.0 0.005 Iso ro •(benzene ND 005 4-Iso ro d toluene ND 1.0 0.005 Metbvl-t-bra I ether MTBE ND 005 Meth (ene chloride ND LO (1.005 4-Meth •I emanone MIRK ND .U05 Naphthalene ND 1.0 0.005 Nitrobenzene ND .1 n-Propyl I benzene ND 1.0 OA05 Styrene ND .005 ] 1 1 2-Tetrachloroethane ND l.f) 0.005 11.2 2-Tetrachloroetbane ND .005 Tetrachloroethene ND 1.0 0.005 Toluene ND .005 1 2 3-Trichlorobenzene ND 1.0 0.005 i :4-Trichlorobenzene ND .005 1.1 1-Trichloroethane ND 1.0 0.005 1 1 2-Trichloroethane ND .o05 'rrichloroethene ND 1.0 0.005 E].',4-Trmnctb,lbcnzcnc dnrnBuo o etl a e .005 i_ c a oa N L(1 0.005 ') fl i 5- ri etl •Then enc L0 OU5 Surro ate Recoveries 12 %ss, 94 ¢ n, Comments' ' nater and vapor samples are reported in pe L.soil'.ludgesolid sanrp1s,in in,, k,produc!/mltnon-ayucnu. liquid..mPles and all T('1.P A'- SPLP extract= are reported in mg/L,wipe samples in pg'r.iPe_ ND means not detected above the reportine limit;N/A means analyte not applicable to this analysis. 4 surrogate diluted out of range or coclutes with another peak;S)low surrogate due to matrix interference. • h)lighter than water immiscible sheen/product is present it liquid sample that contains greater than--I col.%sediment;j)reporting limit raised due to high organic conleni/matrix interference; k)reporting limit near,but not identical to our standard reporting limit due to variable Encore snmPic weight; m)reporting limit raised due to insufficient sample amount;n)results are reported on a dry weight basis; )see attached narrative. DHS ELAP Certification N° 1644 - Angela Rydebus,Lab Manager