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110 2nd Avenue ' )7,Pacheco,CA 94553-5560 McCampbell AnarN-vcal, Inc. Telephone:941 '41.lf620 Fax:925-798-1622 Website:www.mccampb6ll.com E-mail:main@rnccampbell.com . Cambria Env.Technology Client Project ID: #424-1840-001;Jimco Date Sampled: 05/26/04 Trucking Plaza Date Received: 05/27/04 5900 Hollis St,Suite A Client Contact: Matt Meyers Date Extracted: 05/27/04 Emeryville,CA 94608 Client P.O.: Date Analyzed: 05/28/04 Volatiles Organics by P&T and GUMS(Basic Target List)* Extraction Method: SW5030B Analytical Method: SW8260B Work Order:0405445 _ Lab ID 0405448-OOIA _ Client ID TP-1 Matrix Soil ReportingReporting Compound Concentration* DF Limit Compound Concentration* DF Limit Acetone _ ND 1.0 50 Acrolein(Propenal) ND 1.0 50 Acrylonitrile ND 1.0 20 tert-Am I meth 1 ether{TAME) ND 1.0 5.0 Benzene _ ND 1.0 5.0 Bromobenzene ND 1.0 5.0 Bromochlorom(ethane_ _ _ ND j 1.0 j 5.0 Bromodichloromethane _ ND 1.0 _ 5.0 _Bromoform _ ND 1.0 5.0 Bromomethane ND t 1.0 5.0 2-Butanone(IvIEK) ND 1.0 10 t-But 1 alcohol(TBA) ND 1.0 25 n-But ly benzene ND 1.0 5.0 sec-Butyl benzene ND 1.0 5.0 Cert-Butyl benzene _ ND 1.0 5.0 Carbon Disulfide ND 1.0 5.0 Carbon Tetrachloride _ _ _ ND 1.0 5.0 Chlorobenzene ND 1.0 5.0 Chloroethane ND 1.0 5.0 2-Chloroeth I Vinyl Ether ND 1.0 10 Chloroform ND 1.0 5.0 Chloromethane ND 1.0 5.0 2-Chlorotoluene_ ND 1.0 5.0 4-Chlorotoluene ND 1.0 5.0 Dibromochloromethane ND i LO 1 5.0 l,2-Dibromo-3-chloro ro ane ND LO___5.0 - ---- -- -- - -.---4-- _. 1,2-Dibromoethane(EDB) - ND _ I.0 5.0 Dibromomethane ND 1.0 _ 5 0 1,2-Dichlorobenzene __ ND - 1.0 5.0 1,3-Dichlorobenzene ; ND 1.0 5.0 1,4-Dichlorobenzene- _ _ ND I 1.0 5.0 Dichlorodifluoromethane ND 1.0 5.0 1.1-Dichloroethane ND I 1.0 5.0 1,2-Dichloroethane(1,2-DCA) ND 1.0 5.0 1.1_Dichloroethene _ -- ND 1.0 5.0 cis-1,2-Dichloroethene ND - 1.0 5.0 trans-l_2-Dichloroethene _ ND 1.0 5.0 1,2-Dichloropro ane ND - 1.05.0_ 1,3-Dichloropropane - ND 1.0 5.0 2,2-Dichloro ro ane ND1� 0 5.0 1,1-Dichloropropene ND I 1-.0 5.5.0 cis-1,3-Dichloro ro ene ND 1.0 5.0 trans-1=3-Dichloropropene ND_ -� 1.0 5.0 Diisopropyl ether(DIPE) ND 1.0 5.0 Ethylbenzene ND - 1.0 5.0 �Ethyl tert-butyl ether(ETBE) ND 1.0 5.0 Hexachlorobutadiene ND 1.0 5.0 Hexachloroethane ND 1.0 5.0 2-Hexanone ND_ LO 5.0 Isopropylbenzene ND 1.0 _5.0 t - 4-Isopropyl toluene t ND 1.0 5.0 Meth 1-t-but 1 ether(MTBE) I ND 1.0 _5.0 Methylene chloride I ND 1.0 5.0 4-Methyl-2-pentanone(MIBK) ND 1.0 5.0 Naphthalene--- ND 1.0 5.0 Nitrobenzene ND 1.0 100 n-Proms benzene _ ND 1.0 5.0 Styrene ND j 1.0 5.0 1.1,1,2-Tetrachloroethane ND 1.0 5.0 1,1,2,2-Tetrachloroethane ND 1.0 5.0 Tetrachloroethene ND 1.0 5.0 Toluene ND 1.0 5.0 1.2,3-Trichlorobenzene -_ ND_ I.0 5.0 1,2,4-Trichlorobenzene ND I 1.0 5.0 1,1,1-Trichloroethane ND 1.0 5.0 1,1,2-Trichloroethane ND 1.0 5.0 Trichloroethene ND 1.0 5.0 Trichlorofluoromethane ND 1.0 5.0 1,2,3-Trichloro ro ane ND 1.0 5.0 1,1,2-Trichloro-1,2,2-trifluoroethane ND I 1.0 100 1,2,4-Trimeth Ibenzene ND 1.0 5.0 1,3,5-Trimeth Ibenzene ND 1 1.0 5.0 Vinyl Chloride ND t 1.0 11 5.0 Xylenes ND 1.0 5.0 Surrogate Recoveries(%) %SS 1: 101 %SS2: 102 %SS3: 103 Comments: *water and vapor samples and all TCLP&SPLP extracts are reported inµg/L.,soiUsludge/solid samples inµg/kg, wipe samples inµg/wipe, product/oil/non-aqueous liquid samples in mg/L. ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis. #surrogate diluted out of range or surrogate coelutes with another peak. h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than-1 vol.%sediment,j)sample diluted due to high organic content. DHS Certification No. 1644 ✓ Angela Rydelius,Lab Manager