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110 2nd Avenue South,##D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' http//www mccampbell coin E-mail majn@mccampbelI coin <br />' Advanced GeoEnvironmental Client Protect ID Junco Truck Plaza Date Sampled 02/19/02 <br /> 837 Shaw Road Date Received 02/20/02 <br />' Stockton, CA 95215 Client Contact Bill Little Date Extracted 02/22-02/2502 <br /> Client P O Date Analyzed 02/22-02/2502 <br />' Seven Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 90815 90816 90817 90818 <br /> MW4/02-19- MW5/02-19- MW6/02-19- MW7/02-19- Reporting Limit <br /> Client ID 02 02 02 02 <br />' Matrix W W W W S w <br /> Compound Concentration* ug/kg ug/L <br />' Di-isopropyl Ether(DiPE) ND ND ND ND 50 10 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND ND ND 50 1 0 <br /> Methyl tert-Butyl Ether(MTBE) ND ND ND ND so 1 0 <br /> tert-Amyl Methyl Ether('TAME) ND ND ND ND so 1 0 <br />' tert-Butanol ND ND ND ND 25 50 <br />' Methanol ND ND ND ND 2500 500 <br /> Ethanol ND ND ND ND 250 50 <br /> 1 <br /> Surrogate Recoveries(%) <br />' Dibromofluoromethane 109 108 106 107 <br />' Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/vnpe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,(J)sample diluted due to <br /> high organic content <br /> 1 <br /> . DHS Certification No 1644 Edward Hanulton, Lab Director <br /> I <br />