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110 2nd Avenue South,11D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone:925-798-1620 Fax:925-798-1622 <br /> Z4 Website:www.mccampbell.com E-mail:main@mccampbeil.com <br /> Cambria Env.Technology Client Project ID: #165-1556; Olympian Date Sampled: 02/02/05 <br /> Ripon <br /> 5900 Hollis St, Suite A Date Received: 02/04/05 <br /> Emeryville,CA 94608 Client Contact: Eugene Pak Date Extracted: 02/04105-02107105 <br /> Client P.O.: Date Analyzed: 02104105-02107/05 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GCIMS* <br /> Extraction Meth°d:SW5030B Analytical Method:SW8260B Work Order:0502074 <br /> Lab ID 0502074-0050 0502074-006C 0502074-0070 0502074-008C <br /> Client ID MW-5 MW-6 MW-7 MW-8 <br /> Reporting Limit for <br /> Matrix W W W _ W DF=t <br /> DF I 1 1� 10 S W <br /> Compound Concentration ug/kg pg/L <br /> tert-Amyl methyl ether(TAME) ND ND ND 9.4 NA 0.5 <br /> t-Butyl alcohol(TBA) ND ND ND ND<50 NA 5.0 <br /> 1,2-Dibromoethane(ED$) ND ND ND ND<5.0 NA 0.5 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND<5.0 NA 0.5 <br /> Diisopropyl ether(DIPS) ND ND ND ND<5.t) NA 0.5 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND<5.0 NA 0.5 <br /> Methyl-t-butyl ether(MTBE) 1.4 5.1 i ND 18D NA 0.5 <br /> Surrogate Recoveries(%} <br /> %SS: 98 106 106 102 <br /> Comments i b <br /> " water and vapor samples are reported in gg/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in pg/wipe. <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis. <br /> #surrogate diluted out of range or surrogate coelutes with another peak. <br /> h)lighter than water immiscible sheen/product is present;i)liquid sample that contains greater than•-1 vol.%sediment;j)sample diluted due to high <br /> organic content/matrix interference;k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight;m) <br /> reporting limit raised due to insufficient sample amount;n results are reported on a dry weight basis; see attached narrative. <br /> DHS Certification No. 1644 _ Angela Rydelius,Lab Manager <br />