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FREEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHENIISTS <br /> • Analysis For Volatile Compounds By EPA Method 8260B <br /> Client Sample ID: GMX-9-8.5 Client: Geomatrix Consultants, Inc. <br /> Date Received: 09/24/99 Project: 5650 <br /> Date Extracted: 09/24/99 Lab ID: 909106-10 <br /> Date Analyzed: 09/24/99 Data File: 092413.D <br /> Matrix: Soil Instrument: GCMS 1 <br /> Units: ug/kg (ppb) Operator: YA <br /> ' Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Dibromofluoromethane 106 50 150 <br /> 1,2-Dichloroethane-d4 114 50 150 <br /> ' Toluene-d8 104 50 150 <br /> 4-Bromofluorobenzene 233 J ip 50 150 <br /> Concentration <br /> ' Compounds: ug/kg (ppb) <br /> Methyl t-butyl ether (MTBE) <5 <br /> ' Benzene <5 <br /> Toluene <5 <br /> ' Ethylbenzene <5 <br /> • m,p-Xylene <5 <br /> o-Xylene <5 <br /> ip - Recovery fell outside of normal control limits. Compounds in the sample matrix interfered with the <br /> quantitation of the analyte. <br /> J - Internal standard associated with the analyte is out of control limits. The reported concentration is <br /> ' an estimate. <br /> 1 <br /> ' 11 <br />