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FRIEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> . Date of Report: 09/28/99 <br /> ' Date Received: 09/24/99 <br /> Project: 5650 <br /> ' QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL SAMPLES <br /> FOR VOLATILES BY EPA METHOD 8260B <br /> ' Laboratory Code: 909106-01 (Duplicate) <br /> Relative <br /> ' Reporting Sample Duplicate Percent Acceptance <br /> Analyte Units Result Result Difference Criteria <br /> Methyl t-butyl ether (MTBE) µg/kg (ppb) <5 <5 nm 0-20 <br /> ' Benzene µg/kg (ppb) <5 <5 nm 0-20 <br /> Trichloroethene µg/kg (ppb) <5 <5 nm 0-20 <br /> tLaboratory Code: 909106-01 (Matrix Spike) <br /> Reporting Spike Sample % Recovery % Recovery Acceptance <br /> ' Analyte Units Level Result MS MSD Criteria RPD <br /> Methyl t-butyl ether (MTBE) µg/kg (ppb) 50 <5 92 79 50-150 15 <br /> Benzene µg/kg (ppb) 50 <5 85 76 50-150 11 <br /> '• Toluene µg/kg (ppb) 50 <5 81 74 50-150 9 <br /> ' Laboratory Code: Laboratory Control Sample <br /> Reporting Spike % Recovery % Recovery Acceptance <br /> Analyte Units Level LITS LCSD Criteria RPD <br /> ' Methyl t-butyl ether (MTBE) µg/kg (ppb) 50 92 99 50.150 7 <br /> Benzene 4g/kg (ppb) 50 90 93 50-150 3 <br /> Toluene µg/kg (ppb) 50 86 82 50-150 4 <br /> nm - The analyte was not detected in one or more of the duplicate analyses. Therefore, calculation of <br /> ' the RPD is not applicable. <br /> 1 <br /> ' 35 <br />