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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4McCAlVIPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' bttn.//www mccamobell com E-mail main@mccampbell com <br /> ' Gallardo&Associates Client Project ID #024 99,Western Oil Date Sampled 03/23-03/24/99 <br /> 9417 Kensington Court &Spreading Date Received 03/25/99 <br /> Windsor,CA 95492 Client Contact Rafael Gallardo Date Extracted 03/29/99 <br /> ' Client P 0 Date Analyzed 03/29/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 05878 <br /> Reporting Limit <br /> Client ID B-4W <br /> ' Matrix W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND so 10 <br /> Ethyl tert-Butyl Ether(ETBE) ND 50 1 0 <br /> [Methyl-tent Butyi Ether(MTBE) ND 50 10 <br /> tent-Amyl Methyl Ether(TAME) ND 50 10 <br /> tert-Butanot ND 25 50 <br /> ' Surrogate Recoveries(%) <br /> ' Dibromofluoromethane 96 <br /> Comments 1 <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ' I ND means not detected above the reporting limit,NIA means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> t <br /> DHS Cgrtifivation No 1644 )t+-Edward Hamilton, Lab Director <br /> k <br />