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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 64http//www,mccamI2bell com E-mail matn@mccampbeil com <br /> Upgradient Environmental Client Project ID #99024 3, Gillies Date Sampled 10/05/99 <br /> P O Box 8002 Trucking Date Received 10/06/99 <br /> Stockton, CA 95208 Client Contact Vic Cherven Date Extracted 10/07-10/10/99 <br /> Client P O Date Analyzed 10/07-10/10/99 <br /> Gasolene Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* &BTEX* <br /> EPA methods 5030,modified 8015,and 8020 or 602,California RWQCB(SF Hay Region)method GCFID(5030) <br /> Lab ID Client ID Matrix TPH(g)+ MTBE Benzene Toluene Ethcn en- Xylenes %Recovery <br /> ze Surrogate <br /> 22826 GT-1 W 94,c/,1 ND ND 095 ND 1 3 105 <br /> 22827 GT-2 W 250,g ND ND 076 ND 068 100 <br /> 22828 GT-3 W ND ND ND 077 ND 084 101 <br /> 22829 GT-6 W 51,a 100 19 3 7 ND 21 102 <br /> Reporting Limit unless W 50 ugfL 5 0 0 5 05 05 0 5 <br /> otherwise stated,ND <br /> means not detected above <br /> the reporting limit mg/kg S 1 0 m /lc 005 0 005 0 005 0 005 0 005 <br /> *water and vapor samples are reported in ug/L,wipe samples in ug/wipe,soil and sludge samples in mg/kg,and all TCLP and SPLP extracts <br /> in ug/L <br /> "cluttered chromatogram,sample peak coelutes with surrogate peak <br /> 'The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsible for their <br /> interpretation a) unmodified or weakly modified gasoline is significant, b) heavier gasoline range compounds are significant(aged <br /> gasoline')), c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds having broad <br /> chromatographic peaks are significant,biologically altered gasoline9,e)TPH pattern that does not appear to be derived from gasoline(7),f) <br /> one to a few isolated peaks present,g)strongly aged gasoline or diesel range compounds are significant,h)lighter than water immiscible <br /> sheen is present,i)liquid sample that contains greater than—5 vol %sediment,])no recognizable pattern <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />