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110 2nd Avenue South,#137,Pacheco,CA 94553-5550 <br /> [-4 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> E-mail mCa <br /> ainmccampbell corn <br /> Upgradient Environmental Client Project ID #99013,Gillies Date Sampled 03119-01122199 <br /> Trucking <br /> P 4 Box 8002 Date Received 03/23/99 <br /> Stockton,CA 95208 <br /> Client Contact Vic Cherven Date Extracted 03/23/99 <br /> i <br /> Client P O Date Analyzed 03125-C3/29/99 <br /> Diesel Range(C10-C23)Extractable Hydrocarbons as Diesel <br /> EPA methods modified 8015,and 3550 or 3510,Califomia RWQC6(SF Say Region)method GCFID(3550)or GCFID(3510) <br /> Lab ID Client ID Matrix TPH(d)+ %F-ecovery <br /> St.rrogate <br /> 05647 GT-10-35 5-36' S 37,a 98 <br /> 05648 GT 10-45 5-46' S 840,a,g 103 <br /> 05649 GT-10-50-50 5' S 9300,a 101 <br /> i <br /> 05650 GT-10-57-57 5' S 19,000,a 103 <br /> 05651 GT-11-40 541' S 6500,a 98 <br /> 05652 GT-1 1-46-46 5' S 5500,a 98 <br /> 05653 GT-11-50 5-51' S 18,000,a,g 99 <br /> 05654 GT-1 1-55 5-56' S 13,000,a 99 <br /> 05655 GT-11-705-71 S 740,a,g 102 <br /> 05656 GT-11-85 5-86' S 19,a 101 <br /> 05657 GT-1 1-90 5-91' S ND 99 <br /> 05658 GT-11-96-96 5' S ND 101 <br /> 05659 GT-11-7S 5-76' S 20,a t02 <br /> 05660 GT-1 1-100 5-101' S ND 99 <br /> Reporting Limit unless otherwise W 50 ug/L <br /> stated,ND means not detected above <br /> the reporting limit S 1 0 mg/kg <br /> "water and vapor samples are reported in ug/L,wipe samples.in ug/wipe,soil and sludge samples in mg/kg,and all TCLP I STU 7/SPLP <br /> extracts in ug/L <br /> "cluttered chromatogram resulting in coeluted surrogate and sample peaks,or,surrogate peak is on elevated baseline,or,surrog tte has been <br /> diminished by dilution of original extract <br /> 4The following descriptions of the TPH chromatogram are cursory in nature and McCampbell Analytical is not responsitle for their <br /> interpretation a)unmodified or weakly modified diesel is significant,b)diesel range compounds are significant,no recognizabl.pattern,c) <br /> • aged diesel's is significant),d)gasoline range compounds are significant,e)medium boiling point pattern that does not match diesel(7), f) <br /> one to a few isolated peaks present, g)oil range compounds are significant, h)lighter than water immiscible sheen is preseit, i) liquid <br /> sample that contains greater than—5 vol %sediment. <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />