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EXCELCHEM <br />. ENVIRONMENTAL LABS <br /> 500 Giuseppe Court, Suite 9 <br /> Roseville, CA 95678 <br /> Phone# (916) 773-3664 Fax# (916) 773-4784 <br /> OA/OC REPORT <br /> Attention Mr Vic Cherven TPHd Analyzed 08-16,18-96 <br /> Upgradient Environmental Matrix Water <br /> 1017 26th Street <br /> Sacramento, CA 95816 <br /> Project 96008/Gillies Trucking <br /> TPHd <br /> PPB <br /> Reporting Limit 50 _ <br /> QA/QC PARAMETER <br /> Matrix Blank ND <br /> . PERCENT RECOVERIES <br /> Laboratory Control Spike 73% <br /> Laboratory Control Spike Duplicate 84% <br /> ppb=puts per billion=uglL=microgram per liter <br /> ND=Not detected Compound(s)maybe present at concentrations below the reporting limit <br /> Spikes&Spike Duplicates were each spiked with 5000 ug of diesel standard <br /> ANALYTICAL PROCEDURES <br /> PHU-i otal penuieuri nyurocaroons as diesel(htgn noiltng points)are mc.a.ured bV extraction using EPA Method 3 10 followed by modified EPA <br /> Method 8015 with direct sample injection into a GC equipped with an FID <br /> 08-19-96 <br /> ab story Representative Date Reported <br /> E\CELCH£M ENVIRONMENTAL LABS IS CERTIFIED BY THE SPATE OF CALIFORNIA <br /> DEPARTMENT OF HEALTH SERVICES AS A HAZARDOUS WASTE TESTING LABORATORY <br /> {CeH6cat,on No 17601 <br /> 3 <br />