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110 2nd Avenue South #137 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798 1620 Fax 925 798 1622 <br /> L4 Websde www mccampbell corn E-mail main a mccampbell corn <br /> Upgradlent Environmental Client Project ID #04009, Gilles Trucking Date Sampled 11/09/04 <br /> P O Box 8002 Date Received 11/10/04 <br /> Stockton, CA 95208 Client Contact Vic Cherven Date Extracted 11/11/04 <br /> Client P O Date Analyzed 11/11/04 <br /> Oxygenated Volatile Organics by P&T and GC1 MS* <br /> Fxtraction Method SW5030B Analytical Method SW0260B Work Order 0411153 <br /> Lab ID 0411153-006C 0411153-007C 0411153-008C 0411153-009C <br /> Client ID GT-12 GT-13A GT-13B GT-14A <br /> Reporting Limit for <br /> Matrix W W W W DF=1 <br /> i <br /> DF 1 1 1 1 S W <br /> 1 <br /> Compound Concentration ug/kg pg/L <br /> i <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> t Butyl alcohol(TBA) ND ND ND ND NA 5 0 <br /> 1 2 Drchloroethane(1,2-DCA) ND ND ND ND NA 05 <br /> Dmopropyl ether(D1PE) ND ND ND ND NA 05 <br /> Fthyl tert-butyl ether(ETBE) ND ND ND ND NA 05 — <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %S4 102 102 104 102 <br /> Comments �-c - -- - - - - -- -----i--- ` �-- -- — -- - — _ -��---- <br /> I <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L soil/sludgelsohd samples to pg/kg, wipe samples inµg/wipe, <br /> product/oillnon-aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br /> it surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present 1)liquid sample that contains greater than—1 vol %sediment, )sample diluted due to high <br /> ,organic content <br /> DHS Certification No 1644 Angela Rydeltus,Lab Manager <br />