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AIR TOXICS LTD. <br />' SAMPLE NAME Method Spike <br /> ID#• 0101040-17A <br /> EPA METHOD TO-14 GC/NIS FULL SCAN <br /> File Name 8010742 Date of-Collection NA <br /> DIL!*actor 1.00 Date of Analysis 4MG1 <br /> Det Limit Det Limit <br /> Compound (ppbv) (uG/m3) %Recovery <br /> Benzene 050 1 6 96 <br /> Toluene 050 1 9 92 <br /> Ethyl Benzene 0 50 22 99 <br /> m,p-Xylene 0 50 2 2 101 <br /> o-Xylene 050 2 2 99 <br /> Ethylene Dibromide 0 50 39 95 <br /> Methyl tert-Butyl Ether 2 0 73 95 <br /> I Ethanol 2 0 3 8 93 <br /> tert-Butyl Alcohol 2 0 6 2 115 <br /> Isopropyl ether 2 0 8 5 113 <br />' Ethyl-tert-butyl Ether 2 0 8 5 111 <br /> tert-amyl methyl ether 2 0 8 5 110 <br /> 1,2-Dichloroethane 0 50 2 0 94 <br /> I Methanol 50 66 85 <br /> TPH ref to Gasoline (MW-100) 5 0 21 Not Spiked <br /> Container Type NA - Not Applicable <br /> Method <br /> Surrogates %Recovery Limits <br /> 1,2-Dichloroethane-d4 96 70-130 <br /> Toluene-d8 100 70-130 <br /> 4-Bromofluorobenzene 105 70-130 <br /> I <br /> I <br /> I <br /> 1 <br />' Page 22 <br />