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Sequoia 680 Chesapeake Dave Redwood City CA 94063 (415) 364 9600 FAX(415) 364-9233 <br /> 404 N Wiget Lane Walnut Credo CA 94598 (510) 988 9600 FAX(510) 988 9673 <br /> �I Analytical 819 Striker Avenue Suite 8 Sacramento CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> r�E A Engineering Science&Tech Client Project ID Exxon 7-3942, 83739421307 <br /> f 3468 Mt Diablo Blvd , Ste B-100 Matrix Liquid z5 <br />' �3 Lafayette, CA 94549 <br /> `iAttentlon T Faulkner r Work Order#. 8505983 -01, 03-05,07,9505985- Reported May 23, 1995N <br /> ,� ,.,.r ec••y n,, NrK .,s�vYxcx...5�� .�,x,4�,e.}�ti�er£�+�$",,,. ,...�4rc 'o"r,'.n;`,.ay.,�i'.Y ra, ^^. }i� xir^+,k:"e:H}fi Y>.+°`,n �• pYa,;V:<f <br /> xµ�,V.x„!s` x+tS JSC4}V'r'3a>x4W NAFrm{+�ie�`x�,mxcvx:#a.:<-r2 <br />' QUALITY CONTROL DATA REPORT <br /> Analyte Benzene Toluene Ethyl Xylenes <br />' Benzene <br /> QC Batch#' GC0518958TEX21A GCO51895BTEX21A GC051895BTEX21A GC0518955TEX21A <br /> Analy. Method: EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Prep Method EPA 5030 EPA 5030 EPA 5030 EPA 5030 <br /> Analyst- J Minkel J Minkel J Minkel J Minkel <br /> MS/MSD #: 950598204 950598204 950598204 950598204 <br /> Sample Conc.. N D N D N D N D <br /> Prepared Date: 5/18/95 5/18/95 5/18/95 5/18/95 <br /> Analyzed Date 5/18/95 5/18/95 5/18/95 5/18/95 <br /> Instrument I D.#: GCHP21 GCHP21 GCHP21 GCHP21 <br /> Cone Spiked: 10pg/L 1opg/L 1opg/L 30Ns/L <br /> Result: 8 5 88 88 26 <br /> MS %Recovery: 85 88 88 87 <br /> Dup Result: 89 91 9 2 28 <br /> MSD %Recov• 89 91 92 93 <br /> RPD: 46 34 44 74 <br /> RPD Limit. 0-50 0-50 0-50 0-50 <br /> xv+K YnN ASYfrr'Y+gYk ifv4vxx,ry w�x+rvri4�Nkf'uY N,"}i.Y xy+r v?'*,witi}Yir�3rix w., rr� er..�x � viY r+Y"ivri rvar,}'r 'O�r'?ti UiSr n`J'q�J.4i{x}.S <br />' yi A+^} "Y tr4i'Yi�K nflM�akPPI'��WMY` v{�`yr°b�E� ,A ,.}f iY i O u`4w 4 ♦ 4{ , h 4 vo{xS .r l�'J 'fix v i, r u,nn l v +~~ vJ~~ <br /> ` .^ �[fY4 49,r>; htSa v`6q`'r" $ 'a f'4`l �}YM}'f4 ¢�. O q f tri Sr L� ` urr a v c 4.J.W vxPv yr Oi vrt•444 vvis:.ivilMi.,'.vr.4 <br /> �.• `.:4r,°w.},�2S.i�,ti���ltr `"Fq„a`a..'::�uS'YiT.....,,. nrrFfa..,.:..�a�.•.Arwr.rr}.vx.,,.i::�k`��f�r'L;,c'ra:c�tf ,ccs„fi,�..wni�.`C..,icor.u.w.`,,.EE'ca.at..iV.,r,a.2,,.,,.x'~ <br /> LCS #' - - - <br />' Prepared Date - - - <br /> Analyzed Date- - - - <br /> Instrument I D #. <br /> Conc.Spiked. <br /> LCS Result: - - - - <br />' LCS %Recov: - - - - <br /> MS/M9D_ <br />' LCS 71-133 72-128 72-130 71-120 <br /> Control Limits <br /> Please Note <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> VyPenner <br /> ALYTICAL preparation,and analytical methods employed for the samples The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch <br /> Project Manager "'MS=Matrix Spike,MSD=MS Duplicate, RPD=Relative%Difference 9505983 EEE <1> <br />