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SEQUOIA ANALYTICAL <br /> 680 Chesapeake Drive Redwood City, CA 94063 <br /> (415) 364-9600 • FAX (415) 364-9233 <br /> Blaine Tech Services, Inc Client Project ID Shell, 4445 Pershing Ave Sampled Oct 1, 1993 <br /> 985 Timothy Drrve Sample Matrix Water Received Oct 4, 1993 <br /> San Jose, CA 95133 Analysis Method EPA 5030/8015/8020 Reported Oct 11, 1993 <br /> Attention Jim Keller First Sample # 3J12401 <br /> i <br /> TOTAL PURGEABLE PETROLEUM HYDROCARBONS with BTEX DISTINCTION <br /> Reporting Sample Sample Sample Sample Sample Sample <br /> Analyte Limit I D I D I D. I D. I D I D <br /> Mg/L 3J12401 3J12402 3Ji2403 3J12404 3J12405 3J12406 <br /> MW-1 MW-2 MW-3 MW-4 DUP TRIP <br /> Purgeable <br /> Hydrocarbons 50 62 N D N D 50 60 N D <br /> Benzene 050 N D 0 95 N D 26 29 N D <br /> Toluene 050 N D 24 N D N D N D N D <br /> Ethyl Benzene 050 N D N D N D 066 0 82 N D <br /> Total Xylenes 0 50 N D 32 N D N D N D N D <br /> Chromatogram Pattern Discrete Gas Gas Gas - <br /> Peak <br /> Quality Controi Data <br /> Report Limit Multiplication Factor 1 0 1 0 1 0 1 0 1 0 1 0 <br /> Date Analyzed 10/5/93 10/5/93 10/5/93 10/5/93 10/5/93 10/5/93 <br /> Instrument Identification GCHP-18 GCHP-1 S GCHP-18 GCHP-18 GCHP-18 GCHP-18 <br /> Surrogate Recovery, % 105 92 96 86 100 92 <br /> (OC Limits = 70-130%) <br /> aurgeaole Hydrocarbons are ouantitated against a fresh gasoline standard <br /> Analytes reported as N D were not detected above the stated reoorung limit <br /> EW01A ANALY-TICAL <br /> ki6gyl ,Penner <br /> roirt priager 3J12401 BLA <1> <br /> ti�� <br />