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C0 AMERICAN SCIENTIFIC LABORATORIES, LLC <br /> 0 Environmental Testing Services <br /> ANALYTICAL RESULTS <br /> Page 40 <br /> Project ID 1232 Job Number Order Date t;laent <br /> Project Name Unocal-Stockton 10692 03/29/200] EAI <br /> Method 8260B, Volatile Organic Compounds + Oxygenates <br /> Batch No 041101-1 <br /> Our Lab LI)i 66787 66788 <br /> Sample ID MW-23D MW-24D <br /> Date Sampled 03/28/2001 03/28/2e01 <br /> Analytes PQL Results Results <br /> 1,3,5-Trnnethylbenzene 1 000 16 5 ND <br /> Vinyl acetate 5 00 ND ND <br />' Vinyl chloncle(CMoroethene) 3 000 ND ND <br /> 0-Xylene 1 000 e9 7 ND <br /> m-&p-Xylenes 2 000 167 ND <br /> I <br /> Our Lab LD 66787 66788 <br /> Surrogates Con Lmmit Rec. S Rec <br /> Surrogate Percent Recovery <br /> Bromofluorobenzene 70-120 108 115 <br /> Dibromofluoromethane 70-120 11e 100 <br /> oluene-118 70-120 111 106 <br /> QUALITY CONTROL REPORT <br /> Batch No 041101-1 <br /> MS MS Dt1P RPD MSIMSD 1 MS RPD <br /> Analytes %REG %REG % °,G Limit %Limit <br /> Benzene 119 120 <1 75-120 15 <br /> Chlorobenzene 102 102 <1 75-120 1s <br /> 1,1-Dtchloroethene 120 120 <1 75-120 15 <br /> (1,1-Dachloroethylene) <br /> MTBE 120 106 12 4 75-120 15 <br /> Toluene(Methyl benzene) 11e 120 1 7 75-120 15 <br /> Trichloroethene(Tnchloroethylene) 118 119 <1 75-120 15 <br />' ND-Not Detedod at The Detection Limit. MS-Matrix Spike MSD-Matrix Spike Duplicate SM-Sample SMD-Sample Duplicate <br /> 3225 San Fernando Road, Los Angeles, California 90065 • (323) 254-7700, Fax (323) 254-7799 <br />