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r <br /> s <br /> AMERICAN SCIENTIFIC LABORATORIES, LLC <br /> k.� Environmental Testing Services <br /> ANALYTICAL RESULTS <br /> Page 46 <br /> Project ID 1232 Job Number Order Date Client <br /> Project Name Unocal-Stockton 10692 03/29/2001 EAI <br /> Method 8260B, Volatile Organic Compounds + Oxygenates <br /> Batch No 041101-1 <br /> Our Lab LD 66779 66785 <br /> Sample ID MW-25D MW 11 <br /> Date Sampled 03/28/2001 03/28/2001 <br /> Analytes PQL Results Results <br /> 1,3,5-Trirnethylbenzene 100 766 ND <br /> Vinyl acetate 500 ND ND <br />' Vinyl chlonde(Chloroethene) 300 ria ND <br /> o-Xylene 100 7350 ND <br /> m-&p-Xylenes 200 14000 ND <br /> Our Lab LD 66779 66785 <br /> Surrogates Con L-1--it Rec. S Rec <br />' Surrogate Percent Recovery <br /> Bromofluorobenzene 70-120 111 113 <br /> Dibromofluoromethane 70-120 120 120 <br /> mmo6i'Loluene-d8 70-120 108 iia <br /> QUALITY CONTROL REPORT <br /> Batch No 041101-1 <br /> MS MS DUP RPD MS/MSD MS RPD <br /> Analytes %REC %REC % %Limit %Lima <br /> Benzene 119 120 <1 75-120 15 <br /> Chlorobetzene 102 102 <1 75-120 15 <br /> 1,1-Dichloroethene 120 120 <1 75-120 15 <br /> (1,1-Dtchloroethylene) <br /> MTBE 120 106 12 4 75-120 15 <br /> ' Toluene(Methyl benzene) 118 120 1 7 75-120 15 <br /> Tnchloroethene(Trichloroethylene) 118 119 <1 75-120 15 <br /> p <br /> p <br /> ND-Not Detected at The Detection Limit MS-Matna Spike MSD Matrix Spike Duplicate SM-Sample SMD-Sample Duplicate <br /> ' 3225 San Fernando Road, Los Angeles, California 90065 • (323) 254-7700, Fax (323) 254-7799 <br />