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C0 <br /> +e; i , ; AMERICAN SCIENTIFIC LABORATORIES, LLC <br /> •.� : 1Lull,�► <br /> :. ,.� Environmental Testing Services <br /> ANALYTICAL RESULTS <br /> Page 37 <br /> Project ID 1232 ,lab Number Order Date Client <br /> Project Name Unocal-Stockton <br /> 10448 02/26/2001 EAI <br /> Method 8260B, Volatile Organic Compounds + Oxygenates <br /> Batch No 030901-1 <br /> Our Lab 1D T 65372 65373 1 65374 65377 65378 <br /> Sample ID MW24D-55' MW24D-60' MW24-65' NCW24-80' MW24-85' <br /> Date Sampled 02/23/2001 02/23/2001 02/23/2001 02/23/2001 02/23/2001 <br /> Analytes PQL Results Results Results Results Results <br /> TncMorofluoromethane 10 ND I ND ND ND ND <br /> 1,2,3-Tnchloropropane 10 xn rtD ND ND Nn <br /> 1,2,4-Trunethylbenzene 10 ND ND ND 115 62 <br /> 1,3,5-Tnrnethv1benzene 10 ND ND ND 30 15 <br /> Vinyl acetate 50 ND ND ND ND ND <br /> Vinyl chloride(Chloroethene) 30 Nn ND IM ND ND <br /> o-Xylene 2ND ND ND 21 15 <br /> m-&p-Xvlenea 4 ND ND ND 273 227 <br /> Our Lab LD 65372 65373 65374 65377 65378 <br /> Surrogates Con Lima $ Rec $ Rec $ Rec $ Rec $ Rec <br /> rrogate Percent Recovery <br /> mofluorobenzene 70-120 104 I 104 104 102 101 <br /> Dibromofluoromethane 70-120 92 I 92 91 89 89 <br /> Toluene-d8 70-1z0 9e 100 90 98 se <br /> QUALITY CONTROL REPORT <br /> Batch No 030901-1 <br /> MS MS DUP RPD MSIMSD MS RPD <br /> Analytes % REC % REC % %emit %Limit <br /> Benzene 97 99 2 0 75-120 15 <br /> Chlorobenzene 97 se 1 0 75-120 15 <br /> 1,1-Dtchloroethene 98 106 7 8 75-120 15 <br /> (1,1-Dichloroethylene) <br /> MTBE 90 100 10 5 75-120 15 <br /> Toluene(Methyl benzene) 96 98 2 1 75-120 15 <br /> Tnchloroethene(Trichloroethylene) 98 100 2 0 75-120 15 <br />,ND Not Dete,,ted at The Detection Lima MS-Matrix Spike MSD Manx Spike Dupl,,ate SM-Sample SMD-Sample Duphwate <br /> 3225 San Fernando Road, Los Angeles, California 90065 • (323) 254-7700, Fax (323) 254-7799 <br />