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819 Sinker Ave Ste 8 <br /> Sequoia Sacramento CA 95634 <br /> (916)921-9600 <br /> Analytical FAX(916)921-0 100 <br /> ma I www sequoialabs cam <br /> ettler-Ryan-Dublin Project Unocal 5098,Stockton,CA S210010 <br /> Sierra Court,Ste ] Project Number N/A Reported <br /> n CA,94568 Project Manager Deanna L Harding 10/14/02 18 46 <br /> Total Purgeable Hydrocarbons by DHS LUFT <br /> Sequoia Analytical - Sacramento <br /> Reporting <br /> alyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br /> JJYV-J3 (S2J00J0J5)Water Sampled 09/23/0215 20 Received 09/26/02 18 35 <br /> geable Hydrocarbons ND _ _ _ 50 ug/l 1 2100086 10/05/02 10/07/02 DHS LUFT <br /> Surrogate a,a,a-Trtfluorotoluene 107% 60-140 " <br /> INV-] S210010-16 Water Sampled 09/24/0216 47 Received 09/26/02 18 35 <br /> geable Hydrocarbons ND 50 ug/1 1 2100086 10/05102 ]0/07102 DHS LUFT <br /> Surrogate a a,a-Trifluorotoluene 109% 60-140 " <br /> -14A (S230010-17)Water Sam led 09/24/02 17 27 Received 09/26/02 18 35 <br /> geable Hydrocarbons 910 50 ug/l 1 2100086 10/05/02 10/07/02 DHS LUFT HC-21 <br /> Surrogate aa a-Trifluorotoluene 111 % 60-140 " <br /> 11-15(S210010-18)Water Sampled 09/24/02 18 46 Received 09/26/02 18 35 <br /> Purgeable Hydrocarbons ND 50 ug/I 1 2100086 10/05/02 10/07/02 DHS LUFT <br /> 1ogale a,a,a-Trifluorotoluene 101 % 60-140 11 11 11 <br /> -16(S2]0010-19)Water Sampled 09/23/0212 35 Received 09/26/02 18 35 _ .,...,._._.._.... <br /> Purgeable Hydrocarbons 130 50 ugll 1 2100086 10/05/02 10/07/02 DHS LUFT HC-21 <br /> Pae <br /> a,a-Trifluorotoluene 111 % 60-140 " <br /> (S2I0010-20)Water Sampled 09/22/02 17 23 Received 09/26/02 18 35 ._ H'1'-RS <br /> Pur eable Hydrocarbons 140 50 ug/1 1 2100086 10/05/02 10/07/02 DHS LOFT HC-21 <br /> ogate a a a-Difluorotoluene 105 % 60-140 <br /> =18(5210010-21)Water Sampled 09/23/0214 45 Received 09/26/02 18 35 <br /> PiWeable Hydrocarbons ND 50 UO1 2100087 10/05/02 10/05/02 DHS LUFT <br /> Silogale a a,a-Trifluorotoluene 98% 60-140 <br />)caoia Analytical - Sacramento The results in this repor r apply to the samples analyzed in accordance with the chain of <br /> . custody document Unless otherwise stated r esults are reported on a wet weight basis <br /> This analytical repor t must be reproduced in its entirety <br /> Page 6 of 119 <br />