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Sequoia 819 <br /> Sacramento <br /> Ave <br /> 95834 <br /> Sacramento CA 95834 <br /> � Analytical 916)9219660 <br /> FAX((9i6)921-0100 <br /> www sequotalabs com <br /> ettler-Ryan-Dublin Project Unocal 5098,Stockton,CA 5210010 <br /> Sterna Court,Ste J Project Number N/A Reported <br /> to CA,94568 Project Manager Deanna L Harding 10/14/02 18 46 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical - Sacramento <br /> Reportmg Spike Source %REC RPD <br /> Analyte. Result Limit Units Level Result %RHC Limits RPD Limit Notes <br /> Bltch 2100066-EPA 5030E [P/TJ <br /> ank (2100066-BLKI) Prepared&Analyzed 10/03/02 <br /> Itthyopropyltoluene ND 050 ug/l <br /> l <br /> hylene chloride ND 1 0 <br /> tert-butyl ether ND 050 " <br /> Naphthalene ND 10 " <br /> pylbenzene ND 050 <br /> tcne <br /> ND 050 " <br /> 1,1,1,2-Tetrachloroethane ND 050 " <br /> t,2-Tetrachloroethane ND 10 <br /> chloroethene ND 050 " <br /> Toluene ND 050 " <br /> tTnchlorobenzene ND 050 " <br /> -Trichlorobenzene ND 050 <br /> 1,1,1-Trichloroethane ND 050 " <br /> [chloroethane ND 050 " <br /> ethene ND 050 " <br /> Icohl.r,fluoromethanc - ND 050 " <br /> 12 3-Tnchloropropane ND 10 " <br /> 1 -Tnmethylbenzene ND 0 50 <br /> 11-Tnmethylbenzene ND 0 50 " <br /> VinXI chloride ND 050 " <br />�l Xylenes ND 050 " <br /> surrogate Dibromofluoromethane 245 250 98 70 130 <br /> agate 1 2-DCA-d4 267 250 107 70 130 <br /> agate Toluene d8 286 25 0 114 70-130 <br /> urrogale 4-BFB 279 25 0 112 70 130 <br /> oratory Control Sample(2100066-BSI) Prepared&Analyzed 10/03/02 <br /> lenzene 246 0 50 u8A 25 0 98 70-130 <br /> obenzene 24 5 0 50 250 98 70-130 <br /> fr0 <br /> ichloroethene 24 3 0 50 25 0 97 70-130 <br /> oluene 25 1 050 250 100 70-130 <br /> loroethene 204 050 25 0 82 70-130 <br /> Irrogate Dibromofluoromethane 24 6 250 98 70-130 <br /> gate 12-DCA-d4 266 250 <br /> 106 70-130 <br /> Woia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Unless otherwise stated i esults ai a reported on a wet weight ba vis <br /> This analytical report must be reproduced in its entirety <br /> Page 102 of 119 <br />