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539 Stnkei Ave Sia 8 <br /> Sequoia Sacramerttoertio CA a5g44 <br /> (9 16)921 9600 <br /> Anahlical FAX M6)921 0100 <br /> www ecquoialabs com <br /> *11 <br /> er-Ryan-Dublin Prosect Former Unocal 5098,Sloe],ton,CA 5305190 <br /> Sierra Court Ste J Project Number N/A Reportedin CA, 94568 Project Manager Deanna L Harding 05/21/03 17 32 <br /> Gasolme\BTEX1Oxygenates by EPA method 8260B - Quality Control <br /> Sequoia Analytical - Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result °%REC Limits RPB Limit Notes <br /> tatcb 3050185-EPA 5030B JP/Tl <br /> Labot atery Control Sample(1050185-BSI) Prepared 05/12/03 Analyzed 05/13/03 <br /> Iizelie 249 050 ug/1 25 0 100 70-130 <br /> luene 26 2 0 50 25 0 105 70-130 <br /> Metlnl terl butyl ether 17 2 2 0 25 0 69 60-140 <br /> 4 <br /> r i ogaie 12-DCA d4 26 h' 250 107 60 140 <br /> i rogare Toluene dN 26 7 25 0 107 60 140 <br /> Sui i ogale 4 BFB 788 25 0 75 00-140 <br /> Batch 3050220- EPA 5030B IP/TJ <br /> nl, (3050220-BLJ<I) Prepared 05/13/03 Analv7ed 05/14/03 <br /> izene ND 050 ug/I <br /> Toluene ND 0 50 <br /> ene ND 050 <br /> 0{71 <br /> otal) ND 050 <br /> Methyl ter(butyl ether ND 2 0 <br /> AM <br /> i ogare 12-DC4 d4 284 250 114 60-140 <br /> ra'ate Toluene dh 26 h' 25 0 107 60-140 <br /> Sup r ogare 4-BFB 19 3 25 tl 77 60 140 <br /> laboi alery Control Sample(3050220-BSI) Prepared 05/11/03 Analyzed 05/14/03 <br /> Benzene 25 ; 0,;() ug/] 25 0 101 70-130 <br /> 1uene 24 5 Oso 250 98 70-130 <br /> 111y)ten-butyl ether 206 2 0 250 82 60-140 <br /> Irogare 1 2-,SCA d4 27 3 " 250 109 60-140 <br /> rogaie Toluene dX 26 t 25 O 105 0-140 <br /> Sin rogare 4 BFB 21 A 250 87 66440 <br /> a Analytical - Sam amenio The results in ihrc i epos i apply to the winplee analyzed in accoi dance with ilte chain of <br /> custodrdocurnew Unlessoiheoifsewaied ieaulisarerepotiedonaweiweighihaeis <br /> This analvitcal report must be reproduced in its eniuen <br /> Page 101 of 121 <br />