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KD (9JSequoia S195irilerAse5leA <br /> 6)92i 9600 <br /> Sacramemo Cq 95534 <br /> Analytical FAN f916)921 0100 <br /> wuw ,egoomlabs com <br /> Gettler-Ryan-Dublin Project Former Unocal 5098,Stockton,CA 5305190 <br /> 6747 Sierra Court, Ste J Project Number NIA Repo,ted <br /> Dublin CA,94568 Prosect Manager Deanna L Harding <br /> 05/21!03 17 �2 <br /> Volatile Organic Compounds by EPA Method 8260B - Quality Control <br /> Sequoia Analytical - Sacramento <br /> Reporting Spike Source %REC RPD <br /> lAnalyle Result Limn Units Level Result %REC Limits RPD Limn Note, <br /> Balch 3050185-EPA 5030B IP/Tl <br /> Blank(3050185-BLKI) - Prepared 05/12/03 Analyzed 05/13/03 <br /> Trichloroethene ND 050 up/] <br /> Trichlorofluoromethane ND 0 q " <br /> 1 2 1 Tnchloropropsne ND 1 0 <br /> 1 2 4 Trimethylbenzene ND 050 <br /> 1 1 5-7iimethylberzene ND 050 <br /> Vjml chloride ND 0 50 <br /> XV1Cne5(101a1) ND 0 z0 <br /> Sur i quare 1 2-DCA-d4 26 7 2 5 0 107 ' 40-140 <br /> Surlocaw Drbromofluoromeihane 26 6 25 o 106 70 130 <br /> S117n,are 12DCA44267 250 107 70-131) <br /> Surro,are Toluene-d8 26 9 250 108 70 130 <br /> Surrogate 4-BFB R58 25 0 47 70 130 S IIA <br /> l,aboi aloe v Control Sample(30;01 85-BSI) Prepared 05112/03 Analyzed 05/13/03 <br /> Scnzene 249 0 50 ug/l 25 0 100 70 130 <br />_ CI31or�hen�ene 2a r n cn 2c <br /> - 70 7V-1 V <br /> 11-Dchloroethene 21 4 0 50 25 0 94 70-110 <br />— Tnluene---- 262 050 25 0 105 70-110 - <br /> I nchloroethene- 2 3 2- � _ 0 50 <br />-�'- -- - - -- -- -- -- - r _ <br /> Sur i o,aie 1 1-DCA d4 - - 26 8 - - - - 15 0 107- 60 140 - - <br /> Suri o.oie Dibi omofluoromethane 26 6 25 0 106 70 130 <br /> Swigg,ofe 1 2-DCA d4 26 8 25 0 107 70-130 <br /> Surrogate Tnluene d8 - _ -- - u . _ 26 7 __ __,- _ __ - -251) 107- - 70-130 <br /> Surrogate 4-3FB Ih 8 25 0 75 70.130 <br /> Batch 3050218-EPA 5030B IP/Tl <br /> Blank(3050218-BL,K1) Prepared Analyzed 05/13/01 _ <br /> Ten-butyl alcohol -- --ND —100--ug/] ----- ----- ----- <br /> Di-isopropyl ether ND 2 0 <br /> Ethvl ten-butyl ether ND 2 0 <br /> Ten-amyl methyl ether ND 2 0 <br /> Ethanol - ND - 500- - - - - <br /> 1 2-Dichloioethane ND 2 0 <br /> Sequoia Analytical - Saci arnento The resuhs in this report apph to the samples analvzad to decor dance x rih ibe chum of <br /> cusiodi document Unless others ise stated re,ulfs are repot ted on a Het weight basis <br /> Tlris analrncal ieporl must be repo oduced m its enlirety <br /> Page 1 10 of 121 <br />