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4DSequoia 619 Sn"erAve Sie 5 <br /> Sacramemo C,4,951,34 <br /> Analytical (9)6)921 9(>00 <br /> FAX(916)921 0100 <br /> wx w 4equoralabs corn <br /> Gettler-Ryan-Dublin Project Fonner Unocal 5098,Stockton,CA 5305190 <br /> 6747 Siena Coun,Ste J Project Number N/A Re orted rf <br /> Dublin CA, 94568 P <br /> Project Manager Deanna L hlardmg 05/21/03 17 32 <br /> Volatile Organic Compounds by EPA Method 8260E <br /> Quality Q y Control <br /> Sequoia Analytical - Sacramento <br /> Ana] heReponing Spike Source %REC RPD <br /> Result Limit Units Le, Result %REC Limas RPD Umit Notes <br /> Batch 3050307- EPA 5030B IP/TJ <br /> Blank(3050307-BLK1) _ Prepared & Analyzed 05/19/03-- v <br /> l 2 3-1 nchlorobenzene ND 0 50 ug/l <br /> 1 2 4 1 nchlorobenzene ND 0 q0 i <br /> 1 I,1-1rrchloroelhane ND 0 50 " <br /> 1,1,2-lrrchloroelhane ND 050 <br /> 7 richloroethene ND 050 <br /> s <br /> Trrchl03017110mmethane ND 050 ' <br /> 1 2 1-1 rrchloropropane ND 1 0 <br /> 1 2 4-Trrme1hylbenzene ND 050 <br /> 1 3 5-Tlmieiliy1benzene ND + <br /> 0 50 <br /> VimI chloride ND 0 50 <br /> Avlenec(total) - ND <br /> Surrogate J 1 DCA d4 26 0 25 1) - - <br /> J04 60140 <br /> Surrogate Dibronio/luoroniethmTe 15 1 15() 1D2 70 170 1 <br /> Sur rogate J 2 DCA d4 200 15 1) 104 70 130 <br /> Surrogate Toluene dH 26 7 25 0 107 70 170 <br /> Surrogate 4 BFB 214_ 15 11 l:A <br /> —lraborator��Control-Sample(3050307-BS1} �� Prepared& Analyzed 05/19/03 <br /> Benzene 24 9 _0 50—ug/1--— "25 0--- <br /> _ ___ .. <br /> Chiorobenzene — -- --- ----- - -- i <br /> 24 7 D 50 1 I 2S 0 99 70-]30 <br /> 1-D,chlaroethene--- _ -- --23 5 — -0 50 _ " 250 94 70-1—- -- - _ <br /> Toluene 26 1 050 21 0 <br /> 104 70-1 30 <br /> Trichloroethene 23 4 050 25 0 <br /> 94 70 ]3U <br /> �Surrogore 1 2-DC4 d4 ✓' 260 250 104 60 140 <br /> �1 <br /> Surrogate Dibromofluciomelhane 71') 3 15 0 <br /> 105 70-130 <br /> Sul)ogate 12 DCA d4 115 0 ?5 r1 104 70 130 - <br /> Sur r ogole Toluene-d8 20 7 25 0 107 <br /> 711-170- <br /> Suriovate 4-BFB 27 3 15 0 93 70 130 <br /> Sequoia Analytical - Saciarnento <br /> The i es ults,n dTr r r eporr applV to the samples anolr zed w accordance wrth the cliam of <br /> rustodi document bnles%otherrs rse slated results m e reported on a wet N e,glit Nasi s 0V <br /> Thu anah4tral i eporr must be reproduced in its entu en <br /> Page 12,0 of 121 <br />