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I <br /> 1 <br /> CALIFORNIA LABORATORY SERVICES <br /> 12/16/04 10 02 <br /> I ENSR-Sacramento Project Fortner Unocal 5098,5400 PVcCrvke Or�en1CNL0365 <br /> 10411 Old Placerville Rd,Suite 210 Project Number 06940-293-130 C <br /> Sacramento,CA 95827-2508 Project Manager Ben I Hentngburg <br />' Volatile Organic Compounds by EPA Method 8260B- Quality Control <br />' Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch CN09560-EPA 5030 Water MS <br />' Blank(CN09560-BLKI) Prepared&Analyzed 12/13/04 <br /> 13 5-Trimethylbenzene ND 050 µSIL <br /> Vinyl chloride ND 10 <br />' Xylenes(total) ND 10 <br /> Surrogate 12-Dichloroethane-d4 108 100 108 66-135 <br /> Surrogate Toluene-d8 986 100 986 72-125 <br /> Surrogate 4-Bromofluorobenzene 101 100 102 73-125 <br /> LCS(CN09560-BSI) Prepared&Analyzed 12/13/04 <br /> Benzene 201 0 50 pg/L 200 100 60-135 <br />' Chlorobenzene 19 9 050 200 995 60-133 <br /> Woluene1-Dichloroethene 204 050 20 0 102 42-150 <br /> 205 050 20 0 102 60-137 <br /> Trichloroethene 19 5 050 20 0 975 62-140 <br />' Surrogate 12-Dichloroethane-d4 107 I' 100 107 66-135 <br /> Surrogate Toluene-d8 110 100 110 72-125 <br /> Surrogate 4-Bromofluorobenzene 977 100 977 73-125 <br /> LCS Dup(CN09560-ESDI) Prepared&Analyzed 12/13/04 <br /> Benzene 195 050 ug/L 200 975 60-135 3 03 25 <br /> Chloroberizene 193 0 50 200 965 60-133 3 06 25 <br />' 1 l-Dichloroethcne 189 050 200 945 42-150 763 25 <br /> Toluene 196 050 200 98 0 60-137 4 49 25 <br /> Trichloroethene 193 050 20 0 965 62-140 103 25 <br /> Surrogate 12-Dichloroethane-l4 106 100 106 66-135 <br />' Surrogate Toluene-& 107 I' 100 107 72-125 <br /> Surrogate 4-Bromofluorobenzene 991 100 991 73-125 <br /> ICA DOHS FLAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova, CA 95742 www californtalab coin 916-638-7301 Fax. 916-638-4510 <br />