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es a i .Ih.4 I I' g a't1; 1. WORK ORDER 9710044 QUALITY CONTROL REPORT PAGE QR-7 • ANALYSIS TPH as Diesel MATRIX Water SAMPLE SURROGATES SAMPLE TYPE Sample Client LAB ID 9710044 OlE INSTR RUN GC C\971008000000/23/ INSTRUMENT HP 5890 PREPARED 10/08/97 BATCH ID USEW100897 1 UNITS mg/L ANALYZED 10/09/97 DILUTION 1 000000 METHOD GC FID REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) n Pentacosane (surr) 93 1 100 93 1 65 125 SAMPLE TYPE Sample Client LAB ID 9710044 02E INSTR RUN GC C\971008000000/5/ INSTRUMENT HP 5890 PREPARED 10/13/97 BATCH ID OSLW100897 1 UNITS mg/L ANALYZED 10/14/97 DILUTION 1 000000 METHOD GC FID REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) n Pentacosane (surr) 83 3 100 83 3 65 125 SAMPLE TYPE Sample Client LAB ID 9710044 03E INSTR RUN GC C\971008000000/6/ INSTRUMENT HP 5890 PREPARED 10/13/97 BATCH ID DSEW100897-1 UNITS mg/L ANALYZED 10/14/97 DILUTION 1 000000 METHOD GC FID REF REPORTING SPIKE RECOVERY REC LIMITS {X} RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (9) LIMIT (X) n Pentacosane (surr) 97 9 100 97 9 65 125 . SAMPLE TYPE Sample Client LAB ID 9710044 04E INSTR RUN GC C\971008000000/7/ INSTRUMENT HP 5890 PREPARED 10/13/97 BATCH ID DSEW100897 1 UNITS mg/L ANALYZED 10/14/97 DILUTION 1 000000 METHOD GC FID REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) n-Pentacosane (surr) 91 0 100 91 0 65 125 SAMPLE TYPE Sample Client LAB ID 9710044 05D INSTR RUN GC C\971008000000/8/ INSTRUMENT HP 5890 PREPARED 10/13/97 BATCH IO DSEW100897-1 UNITS mg/L ANALYZED 10/14/97 DILUTION 1 000000 METHOD GC FID REF REPORTING SPIKE RECOVERY REC LIMITS (X) RPD ANALYTE RESULT RESULT LIMIT VALUE (%) LOW HIGH RPO (X) LIMIT (X) n-Pentacosane (surr) 95 8 100 95 8 65 125 •