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s <br />sample must be filtered. All the materials' precautions used in the construction of the <br />sampling train should be observed for filtration apparatus. Vacuum filtration of <br />groundwater samples is not recommended. <br />Water samples for dissolved inorganic chemical constituents (e.g., metals, alkalinity and <br />anionic species) will be filtered in the field. <br />Sample containers vary with each type of analytical parameter. Selected container types <br />and materials are non-reactive with the sample and the particular analytical parameter <br />being tested. Appropriate containers for volatile organics are glass bottles of at least 40 <br />milliliters in size fitted with teflon -faced silicon septa. Sample containers are properly <br />cleaned and sterilized by the certified laboratory according to the EPA protocol for the <br />individual analysis. <br />Various preservatives are used by the certified laboratory to retard changes in samples. <br />Sample shipment from Exceltech to laboratories performing the selected analyses <br />routinely occurs within 24 hours of sample collection. <br />Analytical Procedures <br />The analysis of groundwater samples is conducted in accordance with accepted <br />quantitative analytical procedures. The following four publications are considered the <br />primary references for groundwater sample analysis, and the contracts with the <br />laboratories analyzing the samples stipulate that the methods set out in these publications <br />be used. Please note that procedures used are periodically updated by federal and state <br />agencies, and the certified laboratories amend analysis as required by the update. <br />• Standard Methods for the Examination of Water and Wastewater. 16th Ed., <br />American Public Health Association, et al., 1985. <br />• Methods for Chemical Analysis of Water and Wastes, U.S. EPA, 600/4-79- <br />020, March 1979. <br />• Test Methods for Evaluation of Solid Waste: Physical/Chemical Methods <br />U.S. EPA SW -846,1982. <br />EXCELTECH, INC. <br />Laboratory Procedures <br />Latest Revision: March 28, 1990 <br />