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� V <br /> 1 ll7 2zd Avenue Saulh,ND7,Pacheco,CA y4553-5569 <br /> McCampbell Analytical, nc. Telephone 925.798.1620 Faz 925-798-1622 <br /> I <br /> Website wane mccampbell enm Email'main r"i,mcczmpbell,com <br /> QC SUMMARY REPORT FOR SW8260B <br /> W.O.Sample Matrix: Soil QC Matrix: Soil WorkOrder: 0602166 <br /> EPA Method:SW8260B Extraction:SW5030B BatchlD:20234 Spiked Sample ID 0602144-001A <br /> Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria{%) <br /> Analyte <br /> mg/Kg mg/Kg °h Rec. %Rec. %RPD %Rec. %Rec. %RPD MS I MSD LCS I LCSD <br /> teri-Amyl methyl ethe r('I'AME ND 0,050 1(4 101 2.22IO1 9R.4 2 31 70- 130 70- 130 <br /> Benzene ND 0.050 110 )09 0.661 111 106 4,52 70- 130 70- 130 <br /> t-Butyl alcohol(TBA) ND 0.25 98.4 96 6 1 91 91 5 67.2 4.80 70- 130 70- 130 <br /> Chlorobenzene ND 0.050 117 1 1 1 S. 994 102 2.60 70- 130 70- 130 <br /> 1,2-Dibromoethane(6D13) ND 0.050 106 106 0 91.4 87.9 3.88 70- 130 70- 130 <br /> 1,2-Dichloroethane(1,2-DCA) ND 0.050 101 102 0.8118 101 98.4 2.47 70- 130 70- 130 <br /> l,l-Dichloroelhene ND 0.050 112 115 2-53 105 103 1 83 70- 130 1 70- 130 <br /> Ditsopropyl ether(!)IPE) ND 0.050 95.4 92,4 3 22 t0] 102 1 37 70- 130 70- 130 <br /> Ethyl cert-butyl ether(F-TBF.) ND 0.050 94.5 93.8 0.778 96.1 942 1.99 70- 130 70- 130 <br /> Methyl-t-butyl ether(M fBl:} ND 0,050 98.3 98.5 0.214 96,8 93.7 3.25 70- 130 70- 130 <br /> Toluene NI) 0.050 1 98 3 101 2 99 94.4 92.4 2.18 70- 130 70- 130 <br /> Trichloroethene ND 0.050 112 112 0 99.9 98 1 88 70- 130 70- 130 <br /> '/ZS 1: 98 0.050 102 98 4.37 98 97 1.57 70- 130 70- 130 <br /> %SS2: 107 0.050 93 94 0,717 94 93 0,692 70- 130 70- 130 <br /> %SS3: 114 0.050 87 89 2.23 91 1 91 0 70- 130 70- 130 <br /> All target compounds in the Method Blank of this extraction batch were NO less than the mciliod Rt,with the following exceptions: <br /> NONE <br /> BATCH 20234 SUMMARY <br /> Sample ID Dale Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 060216f).00 I A 2/08106 2109/06 2109/06 9:49 PM 06021166-002A 2/08106 2109/06 2109/06 t0:31 PM <br /> 0602166-003A 2108106 2109/06 2/09!06 1 1:14 PM <br /> MS=Matrix Spike,MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Peroeni Deviation, <br /> %Recovery-100-(MS-Sample)r(Amount Spiked);RPO=100'(MS- MSD)I((MS+MSD)12). <br /> MS!MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance Criterla due to one or more of the following reasons:a)the sample Is inhomogenous <br /> AND contains significant coneealrations of analyte relative to the amount spiked.or b)the spiked sample's matrix interferes with the spike recovery, <br /> NIA=not enough sample to perform matrix spike and matrix spike duplicate, <br /> NR=analyle concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte <br /> content. <br /> Laboratory extraction solvents such as methylene chloride and acetone may occasionally appear in the method blank at low levels. <br /> DHS Certification No. 1644 QA/QC Officer <br />