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18 July 2008 <br /> AGE-NC Project No. 95-0137 <br /> Page 5 of 6 y <br /> 3.2. COLLECTION OF SOIL VAPOR SAMPLES / <br /> Soil vapor samples will be obtained at a depth of approximately three to four feet bsg in each boring. <br /> Samples will be collected using a Geoprobe soil vapor assembly. <br /> An expendabl6 vapor point will be placed into a point holder at the bottom of an assembly of <br /> 1.25-inch diameter hollow drive rods.The assembly will then be advanced to the specified depth and <br /> retracted approximately six to twelve inches in order to disengage the expendable point and expose <br /> a column of sgata from which soil vapor can be extracted. Single use, '/a-inch diameter disposable <br /> polyethylene tubing is then attached to a tubing adapter equipped with an O-ring to ensure a vacuum- <br /> tight seal. The adapter assembly is then lowered through the center of the hollow drive rods to the <br /> specified depth and secured by threading into the expendable vapor point holder. <br /> Above ground, the surface around the soil vapor sampler will be sealed with a bentonite sealant to <br /> prevent ambicot air intrusion. An isopropyl alcohol (IPA) tracer gas (liquid IPA) will be exposed <br /> within a plastic sheeting over the sampling equipment to detect leakage of ambient air into the <br /> sampling train. The end of the polyethylene tubing is attached by a two-way inlet port to a Tedlar <br /> bag placed inside an SKC Vac-U-Chamber("lung box")vacuum chamber.A vacuum pump attached <br /> to a purge port of the vacuum chamber is then used to purge the exposed soil column, through the <br /> sampling tubing and inlet port, until approximately three volumes of soil vapor or ambient air is <br /> evacuated through the sampling system. The vacuum chamber is then sealed and the vacuum pump <br /> is attached to a vacuum outlet port of the chamber. When vacuum is applied to the chamber, a <br /> negative pressure is created around the Tedlar bag, which inflates, allowing the soil vapor sample <br /> to enter directly into the bag via the inlet port. When the sample is collected,the negative pressure <br /> in the chamber is reduced and the sample bag is sealed,labeled,logged on a chain of custody form, '" <br /> and placed into a dry cooler(cool temperature). Then soil vapor will be collected onto the carbon <br /> coalescent tuba and sealed for semi-volatile analysis(TO 17 analysis),labeled and transported within <br /> a dry cooler. <br /> Subsequently,,all of the collected soil vapor samples and carbon media will be delivered to a State <br /> of California-certified laboratory for analysis of the chemical constituents listed in Section 2.2. All <br /> soil vapor samples will be analyzed within 72 hours of the sampling time. <br /> After collection of the sample, soil vapor from the polyethylene tubing will be monitored for the <br /> presence of volatile organics using a photo-ionization detector(PID)pre-calibrated to isobutylene. <br /> Advanced GeoEnvironmental,Inc. <br />