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2nd 1+tnuL ic,uAI Pd11161V C A 94551 -60 <br /> 1'� <br /> A cCampbell Analytical, Inc. T,hplium W,795 100 ray 925 799 ,622 <br /> 41cbhm wwX+nxLantoNllwm I mail uwm�cnusanipUrlic�ui <br /> QC SUMMARY REPORT FOR E300A <br /> W 0 Sample Matrix Water QC Matrix Water WorkOrder 0603102 <br /> EPA Method E300 1 Extraction E300 1 BatchlD 20594 Spiked Sample ID NIA <br /> Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria{%) <br /> mglL mg1L %Rec % Rec %RPD _ %Rec j % Rec RPD MS 1 MSD LCS/LCSD <br /> Nitrate as IN N/A t NIA N/A N'A 86 972 122 N/A 85 115 <br /> %SS NIA 0 10 N/A N/A NIA 99 97 212 N/A 90 115 <br /> All target compounds in the Method Blank of this extraction batch wereND leas than the method Rt with the tollowing exceptions <br /> NONF <br /> BATCH 20594 SUMMARY <br /> Sample ID Date Sampled Date Extracted Date Analyzed Sample ID Date Sampled Date Extracted Date Analyzed <br /> 0403102-001A 3'07106 10 10 AM 3108106 3/U8106 6 07 PM i 0603102-002A 3107/06 10 50 AM 3108/06 3108106 6 36 AM <br /> 0603102 003A 3/07106 11 10 AN1 3108106 3/08/06 7 04 PM <br /> 0 <br /> MS=Matrix Spike,MSD=Matrix Spike Duplicate LCS=Laboratory Control Sample LCSD=Laboratory Control Sample Duplicate RPD=Relative Percent Deviation <br /> %Recovery=100'(MS Sample)!(Amount Spiked) RPD=100`(MS- MSD)I((MS+MSD)12) <br /> MS I MSD spike recoveries and I or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is Inhomogenous AND <br /> contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery <br /> NIA=not applicable to this method <br /> I <br /> NR=analyte concentration In sample exceeds spike amount for soil matrix or exceeds 2c spike amount for water matrix or sample diluted due to Ilgh matrlx or analyte content <br /> a,s Cettification No 1644 QA/QC Officer <br />