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tIo Ond \venin >(1uIh 4U, i'aLIMU) cA `)4atii :,00_l4 1�c Campbell Analytical, Inc. TLkphwvlc 9�s ,ah I010 rjt ,i+, /=ss 1622 liLUmuL wH« IMLaJupi,cllLuu, h-oiil mainlainiccimpbLllWin i QC SUMMARY REPORT FOR E300.1 W O Sample Matrix Water QC Matrix Water WorkOrder 0604103 EPA Method E300 1 Extraction E300 1 BatchlD 21111 Spiked Sample ID NIA i I Analyte Sample Spiked MS I MSD MS MSD LCS LCSD LCS-LCSD Acceptance Crite na (%) mglL mg/L %Rec % RBC % RPD %Rec I % Rec %RPD MS I MSD LCS 1 LCSD Nitiate As N N/A I NIA NIA N/A 879 885 0 659 NIA 85- I l5 %b5 NIA 0 10 NIA N/A NIA 92 92 0 NrA 90-115 All target uimpoands in the Method Blank of this extraction bati,h were ND less than Lhe method RL with thi-following exceptions NONE BATCH 21111 SUMMARY Sample ID Date Sampled Date Extracted Date Analyzed Sample 0 Date Sampled Dale Extracted Date Analyzed 0604103-001 A 4146106 9 23 AM 4107106 4107106 6 57 PM 10604103 002A 4106/06 9 46 AM 4/07106 4/08106 2 08 AM 0604103-003A 4/06106 10 06 AM 4/07/06 4107'06 7 54 PM 0604103 004A 4/06106 10 36 AM 4/07/06 4'07M6902 AM 0604103-005A 4/06/06 10 51 AM 4/07106 4107106 9 30 PM • MS=Matrix Spike,MSD=Matrix Spike Duplicate,LCS=Laboratory Central Sample LCSD=laboratory Control Sample Duplicate,RPD=Relative Percent Deviation %Recovery=1 DO'(MS-Samplo)I(Amount Spiked) RPD=100"(MS MSD)I((MS+MSD)/2) MS I MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons a)the sample is inhomogenous AND Contains significant concentrations of analyte relative to the amount spiked orb)the spiked sample's matrix interferes with the spike recovery NIA=not applicable to this method NR=analyte concentration In sam le exceeds spike amount for soil matrix or exceeds 2x spike amount for water matnx or sample diluted dhaft h1 h matrix or analyle content 66S Certification No 1644 QVQC Officer