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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' http 1/www mccamnbell,com E-mail main@mccampbell com <br /> • <br /> ' Advanced GeoEnvuonmental Client Project ID Ripon Farm Service Date Sampled 05/11/98 <br /> 4005 North Wilson Way Date Received 05/14/98 <br /> ' Client Contact Bill Little Date Extracted 05/14/98 <br /> Stockton,CA 95205 <br /> Client P Q Date Analyzed 05115-05117198 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab ID 89247 <br /> Client ID B 19-20 <br /> Matrix S <br /> ' Compound Concentration* Compound Concentration* <br /> AcetoneND<400 Ethylbenzene 8500 <br /> Benzene 880 Hexachlorobutadiene ND<400 <br /> ' Bromobenzene ND<400 lodomethane ND<400 <br /> Bromochloromethane ND<400 Isopropylbenzene ND<400 <br /> Bromodichloromethane ND<400 p-Isopropyl toluene ND<400 <br /> Bromoform ND<400 Methyl butyl ketone ND<400 <br /> ' Bromomethane ND<400 Methylene Chlonde"' NIK400 <br /> n-Butyl benzene 2000 Methyl ethyl ketone ' ND<400 <br /> sec-Butyl benzene 470 Methyl isoburyl ketone'g ND<400 <br /> tent-Butyl benzene 1700 Methyl tert-Butyl Ether(MTBE) --- <br /> ' Carbon Disulfide ND<400 Naphthalene 2600 <br /> Carbon Tetrachloride NIK400 n-Propyl benzene 2000 <br /> Chlorobenzene ND<400 Styrene` ' ND<400 <br /> Chloroethane ND<400 1,1,1.2-Tetrachloroethane ND<400 <br /> 2-Chloroethyl Vinyl Ether` ND<400 1,1 2,2-Tetrachloroethane ND<400 <br /> Chloroform ND<400 Tetrachloroethene ND<400 <br /> Chloromethane ND<400 Toluene" ND<400 <br /> 2-Chlorotoluene NDc400 1,2 3-Trichlorobenzene NDX400 <br /> t 4-Chlorotoluene ND<400 1,2 4-Trichlorobenzene ND<400 <br /> Dibromochloromethane ND<400 1 1,1 Trichloroethane ND<400 <br /> 1,24Dibromo-3-chloropropane ND<400 1,1,2 Trichloroethane ND<400 <br /> Dibromomethane ND<400 Trichloroethene ND<400 <br /> 12-Dichlorobenzene ND<400 Tnchlorofluoromethane ND<400 <br /> 1,3-Dichlorobenzene ND<400 1,2,3-Tnchloropropane ND<400 <br /> 1,4-Dichlorobenzene ND<400 1,2 4-Tnniethylbenzene 12,000 <br /> Dichlorodifluoromethane ND<400 1,3,5-Tnmethylbenzene 4400 <br /> ' 1,1-Dichloroethane ND<400 Vinyl Acetate""' ND<400 <br /> 1,2-Dichloroethane ND<400 Vinyl Chloride ND<400 <br /> ]J-Dichloroethene ND<400 Xylenes,total 9100 <br /> cis-1,2-Dichloroethene ND<400 <br /> ' trans-1,2-Di chloroethene ND<400 <br /> 1,2 Dichloropropane ND<400 <br /> 1,3-Dichloropropane ND<400 <br /> 2,2-Dichloropropane ND<400 Comments <br /> ' 1,1-Dichloropropene ND<400 Surrogate Recoveries(%) <br /> cts-1,3-Dichloropropene ND<400 Dibromofluoromeihane 93 <br /> trans-1,3-Dichloropropene ND<400 Toluene-d8 92 <br /> Ethylene dibromide ND<400 4-Bromofluorobenzene 87 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in uglkipe and all TCLP 1 SPLP extracts to ug/L <br /> Reporting limits unless otherwise stated water samples 0 5 ug/L, vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg, wipes <br /> 0 2uglwipe ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> ' (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (0 2-butanone, (g)4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Cernficanon No 1644 Edward Hamilton,Lab Director <br /> 1 <br />