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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httn I/www mccampbell com E-mail main@mccampbell cam <br /> Advanced GeoEnvironmental Client Project ID Ripon Farm Service Date Sampled 05/11/98 <br /> ' 4005 North Wilson Way Date Received 05/14/98 <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 05/14/98 <br /> Client P O Date Analyzed 05/15-05/17/98 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br /> Lab 1D 89249 <br /> Client ID B 19-35 <br /> Matrix S <br /> ' Compound Concentration* Compound Concentration* <br /> Acetone` ND<35 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone" ND <br /> sec-Butyl benzene ND Methyl isobutyi ketone`s ND <br /> tert-Butyl benzene ND Methyl ten-Butyl Ether(MTBE) --- <br /> lieCarbon Disulfide ND Naphthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene' ' ND <br /> Chloroethane ND 1,1,1 2-Tetrachloroethane ND <br /> ' 2-Chloroethyl Vinyl Ether" ND 1 1 2 2-Tetrachloroethane ND <br /> Chloroform ND Tetrachlorocthene ND <br /> Chloromethane ND Toluene' ND <br /> 2-Chlorotoluene ND 1,2,3-Tnclilorobenzene ND <br /> 4-Chlorotoluene ND 1 2,4-Tnchlorobenzene ND <br /> Dibromochloromethane ND 1 l 1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,12-Tnchioroethane ND <br /> Dibromomethane ND Trichioroethene ND <br /> ' 1 2 Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3 Dichlorobenzene ND 1,2 3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2 4-Tnmethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Tnmethylbenzene ND <br /> ' 1 I Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"' ND <br /> 1,1-Dichloroethene ND Xylenes,total '°' NI) <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1 3-Dichioropropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis 1,3-Dichloropropene ND Dibromofluoromethane 97 <br /> trans-1,3-Dichloropropene ND Toluene-d8 96 <br /> Ethylene dibromide ND 4-Bromofluorobenzene 98 <br /> -water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes m uglwipe and all TCLP/SPLP extracts m ug/L <br /> Reporting limits unless otherwise stated water samples 0 5 ug/L vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg wipes <br /> 0 2ug/wipe ND means not detected above the repartmg limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloromethane (t) 2-butanone (g)4-methyl-2- <br /> pentanone or isopropylacetone,(h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes; <br /> ' DHS Certification No 1644 Edward Hamilton, Lab Director <br />