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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hM/lwww_mcc�corn E-mail main@mccampbell com <br /> Advanced GeoEnvironmentalDate Sampled 05/29/98 <br /> Client Project 1D Ripon Farm Service <br /> Date Received 06/02/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Bill Little Date Extracted 06/04-06/05198 <br /> Client P O Date Analyzed 06/04.06105/98 <br /> Volatile Organics By GC/MS <br /> EPA method 9260 <br /> ' Lab ID 89909 <br /> Client ID VW2 /5-29-98 <br /> Matrix W <br /> 1 Compound Concentration' Compound Concentration' <br /> AcetoneND<15 Ethylbenzene 260 <br /> Benzene 30 Hexachlorobutadiene ND<5 <br /> Brorriobenzene ND<5 lodomethane ND<5 <br /> Bromochloromethane ND<5 Isopropylbenzene 33 <br /> Bromodichloromethane Nl><5 p-Isopropyl toluene ND<5 <br /> Bromoform ND<5 Methyl butyl ketone' ND<5 <br /> Bromomethane ND<5 Methylene Chloride` ND<5 <br /> ' n Bury]benzene 18 Methyl ethyl ketone ' ND<5 <br /> sec-Butyl benzene 65 Methyl isobutyl ketone'x ND<5 <br /> tert-Butyl benzene 36 Methyi ten-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<5 Naphthalene 310 <br /> • Carbon Tetrachloride ND<5 n-Propyl benzene 110 <br /> Chlorobenzene ND<5 Styrene' ND<5 <br /> Chloroethane ND<5 1,1 1 2-Tetrachloroethane ND<S <br /> 2-Chloroethyl Vinyl Ether"i ND<5 1,1 2 2-Tetrachloroethane ND<5 <br /> Chloroform ND<5 Tetrachloroethene ND<5 <br /> Chloromethane ND<5 Toluene"' ND<5 <br /> 2-Chlorotoluene ND<5 1,2,3-Tnchlorobenzene ND<5 <br /> ' 4-Chlorotoluene ND<5 1 2 4-Tnchlorobenzene ND<5 <br /> Dibromochloromethane ND<5 1,I,1-Trichloroethane ND<5 <br /> 1,2-Dibromo-3-chloropmpane ND<5 1,1,2-Tnchloroethane NIK5 <br /> Dibromomethane ND<5 Tnchloroetbene ND<5 <br /> ' 1,2-Dichlorobenzene ND<5 Trichlorofluoromethane ND<5 <br /> 1,3-Dichlorobenzene ND<5 1,2,3-Trichloropropane ND<5 <br /> 1,4-Dichlorobenzene ND<5 1,2,4-Trimethylbenzene 390 <br /> Dichlorodifluoromethane ND<5 1,3,5-Trimethylbenzene 110 <br /> I,1-Dichloroethane ND<5 Vinyl Acetate"" ND<5 <br /> 1,2-Dichloroethane 190 Vinyl Chloride"" ND<5 <br /> I,1-Dichloroethene ND<5 Xylenes,total 10j 320 <br /> cis-1,2-Dicbioroethene ND<5 <br /> trans-l,2-Dichloroethene ND<5 <br /> 1,2-Dichloropropane ND<5 <br /> 1,3-Dichloropropane ND<5 <br /> 2,2-Dichloropropane ND<5 comments <br /> i,1-Dichloropropene ND<5 Surrogate Recoi eries{%) <br /> cis-] 3-Dichloropropene ND<5 Dibromofluoromethane 109 <br /> trans-1,3-Dichloropropene ND<5 Toluene-d8 94 <br /> Ethylene dibromide ND<5 4-Bromofluorobenzene 88 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,i apor samples 0 5ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> • ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone (e)dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte,(1)methylbenzene(m)acetic acid ethenyl ester,(n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 11 Edward Hamilton,Lab Director <br /> 1 <br />