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li <br /> laboratories <br /> Ground Zero Analysts <br /> 1714 Main Street Volatile Organics By GC/MS Date Sampled 10/20/03 <br /> Escalon, CA 95320 Date Received 10121/03 <br /> Method EPA 8260B Date Analyzed 10/27/03 <br /> Proj ID 98-263 <br /> Site Tuleburge Warehouse <br /> Matrix Water <br /> Lab ID D10451 D10452 D10453(d) D10454 <br /> Sample ID TW-MW-10 TW-MW-11 TW-MW-12 TW-MW-14B <br /> Units ug1L ug/L ug1L ug1L <br /> Methanol(MeOH) <250 <250 <5,000 e250 <br /> Ethanol(EtOH) <100 <100 <2,000 <100 <br /> t-Butanol(TBA) <20 <20 <400 <20 <br /> Methyl-t-Butyl Ether(MTBE) <2 0 <2 0 2,500 <2 0 <br /> Di-Isopropyl Ether(DIPE) <2 0 <2 0 <40 <2 0 <br /> Ethyl-t-Butyl Ether(ETRE) <2 0 <2 0 <40 <2 0 <br /> t-Amyl Methyl Ether(TAME) <2 0 <2 0 <40 <20 <br /> 1,2-Dichloroethane(1,2-DCA) <2 0 <2 0 <40 <2 0 <br /> 1,2-Dibromoethane(EDB) <2 0 <2 0 <40 <2 0 <br /> QA1QC <br /> Surrogate Spike Recovery 88% 90% 89% 87% <br /> Note(s) <br /> (d) Sample diluted due to high concentration of target analytes and/or high organic content <br /> Water samples are reported in ug/L,sodlsludge samples in mg/Kg,product/oil/non aqueous liquid samples in mg1L <br /> ND means not detected at or above the stated reporting limit,N/A means analyte not applicable to this analysis <br /> �L— L± <br /> Hiram Cueto <br /> Lab Director <br /> DHS Certification No 2359 <br /> i <br /> I <br /> 3037 Fifth St , Ceres, CA 95307 • Phone (209) 581-9280 • Fax (209) 581-9282 <br />