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1 July 16, 2004 Lab ID SP 406522 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic ' Constituent Method Date/1D Type Units Conc QC Data DQO Note ' Hexachlorobutadtene 5242 07/02/2004 A209 BS ug/L 1000 98 3% 73-154 BSD ug/L 10 00 112% 73-154 BSRPD ug/L 129% 515 8 ' 5242 07/02/2004 A 00-CCV ug/L 1000 111% 70-130 Isopropylbenzene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 95 4% 88-143 BSD ug/L 1000 103% 88-143 ' BSRPD ug/L 75% S 17 0 5242 07/02/2004 A 00-CCV ug/L 10 00 101% 70-130 ' p-Isopropyltoluene 5242 07/02/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 950% 88-153 BSD ug1L 1000 115% 88-153 BSRPD ug/L 18 8% 514 8 410 ' 5242 07/02/2004 A 00-CCV ug/L 10 00 104% 70-130 Methyl cert Butyl Ether (MTBE) 5242 07/02/2004 A209 Blank ug/l, ND <1 BS ug/L 1000 110% 62-143 BSD ug/L 1000 74 5% 62-143 BSRPD ug/L 38 5% 517 6 410 5242 07/02/2004 A 00-CCV ug/L 1000 95 7% 70-130 ' Naphthalene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 135% 63-165 BSD ug/L 1000 945% 63-165 BSRPD ug/L 350% 5 30 6 410 ' 5242 07/02/2004 A 00-CCV ug/L 1000 120% 70-130 n-Propylbenzene 5242 07/02/2004 A209 Blank ug/L ND <0 5 ' BS ug/L 1000 908% 85-152 BSD ug/L 1000 101% 85-152 BSRPD ug/L 105% 5 15 6 5242 07/02/2004 A 00-CCV ug/L 1000 96 8% 70-130 ' Styrene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 990% 85-149 BSD ug/L 1000 874% 85-149 ' BSRPD ug/L 124% 516 8 5242 07/02/2004 A 00-CCV ug/L 1000 101% 70-130 Ten amyl methyl Ether (TAME) 5242 07/02/2004 A209 Blank ug/L ND <3 ' BS ug/L 1000 104% 67-129 BSD ug/L 1000 727% 67-129 BSRPD ug/L 3 2 53 00 410 5242 07/02/2004 A 00-CCV ug/L 1000 95 8% 70-130 1 1 1 2-Tetrachloroethane 5242 07/02/2004 A209 Blank ug/L ND <05 Report continued on next page SP 406522 Quality Control Page 6 1