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July 16, 2004 Lab ID SP 406520 ' Ground Zero Analysis Customer 3-14996 Quality Control - Organic ' Constituent Method Date/ID Type Units Cone. QC Data DQO Note ' i-lexachlorobutadiene 5242 07/02/2004 A209 BS ug/L 1000 993% 73-154 BSD ug/L 1000 112% 73-154 BSRPD ug/L 129% 515 8 5242 07/02/2004 A 00-CCV ug/L 1000 111% 70-130 ' isopropylbenzene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 95 4% 88-143 BSD ug/L 1000 103% 88-143 ' BSRPD ug/L 7 5% 517 0 5242 07/02/2004 A 00-CCV ug/L 1000 101% 70-130 p-Isopropyltoluene 5242 07/02/2004 A209 Blank uglL ND <05 BS ug/L 1000 950% 88-153 BSD ug/L 1000 115% 88-153 BSRPD ug/L 18 8% 514 8 410 ' 5242 07/02/2004 A 00-CCV ug/L 1000 104% 70-130 Methyl ten-Bury[ Ether (MTBE) 5242 07/02/2004 A209 Blank ug/L ND <1 BS ug/L 1000 110% 62-143 BSD ug/L 1000 745% 62-143 BSRPD ug/L 38 5% 517 6 410 5242 07/02/2004 A 00-CCV ug/L 1000 95 7% 70-130 Naphthalene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 135% 63-165 BSD ug/L 1000 945% 63-165 BSRPD ug/L 35 0% 530 6 410 5242 07/02/2004 A 00 CCV ug/L 1000 120% 70-130 n Propylbenzene 5242 07/02/2004 A209 Blank ug/L ND <05 BS ug/L 1000 90 8% 85-152 ' BSD ug/L 1000 101% 85-152 BSRPD uglL 105% 515 6 5242 07/02/2004 A 00-CCV ug/L 1000 968% 70-130 ' Styrene 5242 07/02/2004 A209 Blank ug/L ND <0 5 BS ug/L 1000 990% 85-149 BSD ug/L 1000 87 4% 85-149 BSRPD ug/L 124% 516 8 ' 5242 07/02/2004 A 00-CCV ug/L 1000 101% 70-130 Teri-amyl-methvl Ether (TAME) 5242 07/0212004 A209 Blank ug/L ND <3 BS ug/L 1000 104% 67-129 BSD ug/L 1000 727% 67-129 BSRPD ug/L 3 2 53 00 410 524 2 j 07/02/2004 A 00-CCV ug/L 1000 958% 70-130 1 1 1 2-Tetrachloroethane 5242 07/02/2004 A209 Blank ug/L ND <05 Report continued on next page SP 406520 Quality Control Page 6