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1 <br /> 1, <br /> laboratories <br /> • Ground Zero Analyses <br /> 1 1714 Main Street <br /> Escalon, CA 95320 Blank 1 QC Data Date Analyzed 12/18/03 <br />' Prol ID 98 263 Method EPA 8260B <br /> Site Tuleburg Warehouse <br /> Matrix Water <br /> Lab ID BLKD1218 Method Rep Lim <br /> Sample ID Blank Water Soil <br /> Units ug/L ug1L mglKg <br />' Methanol(MeOH) <250 250 050 <br />' Ethanol(EtOH) <100 100 0 025 <br /> t-Butanol(TBA) <5 0 — 50 0 050 <br />' Methyl-t-Butyl Ether(MTBE) <0 5 05 0 005 <br /> Di-Isopropyl Ether(DIPE) <0 5 05 0 005 <br />' Ethyl-t-Butyl Ether(ETBE) <0 5 05 0 005 <br /> lie <br /> t-Amyl Methyl Ether(TAME) <0 5 05 0 005 <br /> 1,2-Dichloroethane(1,2-DCA) <0 5 05 0 005 <br /> t1,2-Dibromoethane(EDB) <0 5 05 0 005 <br />' QA1QC <br /> Surrogate Spike Recovery 97% <br /> Matrix Spike Recovery Summary <br /> Percent Recovery <br />' Lab ID Client ID Analyte MS 1 MSD %RPD <br /> ' D12348 TW MW-9B 1,2-DCA 991102 3 <br /> ' Laboratory Control Spike Recovery Summary <br /> Lab ID Analyte Percent Recovery <br /> LCS1218D TBA 95 <br /> Note(s) <br /> Water samples are reported in ug1L,soil/sludge samples in mg/Kg,product/oil/non aqueous liquid samples in mg/L <br /> ' ND means not detected at or above the stated reporting limit,NIA means analyte not applicable to this analysis <br /> 3037 Fifth St , Ceres, CA 95307 Phone (209) 581-9280 o Fax (209) 581-9282 <br />